@OwlTech333 of course, it's so hard to get nice Pd sometimes but I will have to try the borax to stop oxidation as it's cooling trick I just learned from this video. Thanks
@@OwlTech333 شكراً للرد …. لكن اسمح لي بالتوضيح اكثر من بعد اذنك … قمت بإضافة ماء ساخن إلى إحدى العينات الترابية و بعد الفلترة وجدت أن الماء قد انصبغ باللون الأصفر .. فقمت بتبخير الماء و وجدت اني قد تحصلت على ملح اعتقد انه ملح البلاديوم . سؤالي الان هل فعلاً من الممكن ان يذوب ملح معدن البلاديوم بالماء فقط بهذه الطريقة ؟؟؟ و هل اذا كلست هذا الملح بعد تبخير الماء عنه يكون قابل للصهر ؟
No specific ratio used, just after adding the formic, add the NaOH on small increments, waiting to react between additions until all yellow salt turns black, then continue boiling for 5-10 minutes and it’s done. You don’t need much reagents - for this reduction I used roughly 50ml formic and 10-15g NaOH
Do you prefer NaOH vs NH3? And which Salt reduces quicker with Alkaline/formic acid, Yellow or Red Brick? I had some delayed issues yesterday reducing ~30 grams of red salt with HN3/Formic Acid. Seemed either not enough heat at first or my NH3/formic solution was to diluted.
Sir how are you I have ground many stones and dissolved them in Aqua Regia (stones with stannous chlorid test show Platinum group metals) after urea adding SMB and some Iron sulphide ten grams dust was received around I once again made Aqua Regia to make pure gold, half of the dust did not dissolve, I do not understand what metal it could be.
Hello, good evening, my name is Diego, I'm from Brazil. do you have email so i can send some questions ?? for example: I have an ammoniacal solution containing palladium .... I added hcl and yellow pd salt precipitated .... IF I TAKE THAT YELLOW SALT AND ADD FORMIC ACID AND THEN GO PUT IN SODIUM HYDROXIDE, WILL IT BE BLACK LIKE THIS ?? .....I WORK WITH RHODIUM, PALLADIUM, GOLD AND SILVER ....IT WILL BE A PLEASURE TO EXCHANGE INFORMATION. HUGS
@@OwlTech333 aww! HTe it when it gets away from us for cheaper than value! I remember when palladium was 10% what platinum was. It was like copper or maybe silver. Now platinum is palladium's junior league metal, like silver is gold's... anyways. Just curious.
![FNAF Into the Pit has A LOT of Unused Graphics | LOST BITS [TetraBitGaming]](http://i.ytimg.com/vi/6YhZCRdipl4/mqdefault.jpg)
Fantastic quality of the refining and melt! 🌟🌟🌟🌟🌟👍
Thank you!
شكرا لك استفدنا منك ❤❤❤
Здоров дружище! Красота!
Спасибо большое!
Залипательное видео, приятно видеть как работает маэстро.
Спасибо за просмотр!
Nice.. Pd is very unique.. sometimes , i feel that palladium metal is alive😅 they expand sometimes. Like a metal sponge
👏👏
Beautiful piece mate 👌
Glad you like it!
@OwlTech333 of course, it's so hard to get nice Pd sometimes but I will have to try the borax to stop oxidation as it's cooling trick I just learned from this video. Thanks
Top você realmente mostra como se faz, parabéns 👏👏👏👏
Привет, красивая палладиевая чернь получилась.
👍
Привет! Спасибо!
Very good videos,thank You Owl Tehc.👍🤗👍
Glad you like them!
Отличная работа!
Спасибо!
جميل جدا جدا روعه تسلم استاذ العزيز بلتوفيق أنشاء آلله تحياتي يا من مصر
Thank you!
Beautiful dude!
Score 👍
Peace Prospector Tripp
Thanks 👍
Very cool glad to see you back😊
More to come!
iridium please...
Professionnel thanks for vidéo
سؤال لو سمحت …
هل يذوب ملح البلاديوم بالماء فقط ؟
و هل اذا كان يذوب فطريقة تحويله الى معدن هي نفس الطريقة في هذا الفيديو ؟
يمكنك تحويل ملح البلاديوم إلى معدن بطريقة تسمى التكليس، لكني أفضل التحويل الكيميائي باستخدام حمض الفورميك.
@@OwlTech333 شكراً للرد ….
لكن اسمح لي بالتوضيح اكثر من بعد اذنك …
قمت بإضافة ماء ساخن إلى إحدى العينات الترابية و بعد الفلترة وجدت أن الماء قد انصبغ باللون الأصفر .. فقمت بتبخير الماء و وجدت اني قد تحصلت على ملح اعتقد انه ملح البلاديوم .
سؤالي الان هل فعلاً من الممكن ان يذوب ملح معدن البلاديوم بالماء فقط بهذه الطريقة ؟؟؟
و هل اذا كلست هذا الملح بعد تبخير الماء عنه يكون قابل للصهر ؟
Hey can we do this procedure with dmg yellow salt ? Please reply
yes
thanks for goood video patron 🌹🌹🌹🌹👍
Thank you for watching!
Hi.What are the ratios of formic acid and sodium hydroxide?
No specific ratio used, just after adding the formic, add the NaOH on small increments, waiting to react between additions until all yellow salt turns black, then continue boiling for 5-10 minutes and it’s done. You don’t need much reagents - for this reduction I used roughly 50ml formic and 10-15g NaOH
سلام عليكم عندي بلاديوم اصفر كيف تحويله الئ بلاديوم هل ضيف عليه نتريك ام ماذا ارجو الرد
With formic acid
مرحبا اخي فيديو رائع اخي هل ينطبق الامر على البلاتين كذلك بعد ترسيب ب كلوريد المونيوم التحويله الى اكسيد جاهز الصهر لك شكر وتقدير ❤
Ok
Hi Mr owl, good?
The yellow salt is come from? Please.
MLCCS
Hello, greetings to you for the wonderful effort, sir. I have a group of platinum mixed with sand, which is chloride. How do I start working on it?
😑 why did speed up the video when melting! How much didt tooked?
5min
@@OwlTech333 i melted palladium in less than one minute with arc but the carbon electrodes are a mess. Now i have rhodium 🤞
لو سمحت يافنان الفيديو نازل من غير ترجمة من فضلك اعد صياغة الفيديو بالترجمة
Отличная работа👍 раньше плавил без буры или я ошибаюсь?
Спасибо! Тоже с буры плавил
@@OwlTech333 Я палладий плавлю с содой Na2CO3
Rất hay! Cảm ơn bạn!
So beautiful video I like it❤❤❤
Good job you prof thanks for video
Thanks for watching!
Hello, very good job!
I am converting the yellow salt using HCL and zinc, have you ever tried it?
Yes
Do you prefer NaOH vs NH3? And which Salt reduces quicker with Alkaline/formic acid, Yellow or Red Brick? I had some delayed issues yesterday reducing ~30 grams of red salt with HN3/Formic Acid. Seemed either not enough heat at first or my NH3/formic solution was to diluted.
Hi! Prefer NaOH, never reduced the red salt before so I don't know. As for you issues, heating to at least 85C is a must.
Sir how are you I have ground many stones and dissolved them in Aqua Regia (stones with stannous chlorid test show Platinum group metals) after urea adding SMB and some Iron sulphide ten grams dust was received around I once again made Aqua Regia to make pure gold, half of the dust did not dissolve, I do not understand what metal it could be.
فيديو رائع
Qual foi o processo para obter o sal amarelo de paládio
There’s a video
Здравствуйте!
Отлично!
Скажите, какую музыку используете в ролике?
Спасибо! Музыка моя: on.soundcloud.com/awc6F
Very nice button!
I couldnt see the weight... ill guess maybe a little high, around 11g.
Great vid OwlTech.
9.48g
@@benlee4940 thanks.
9.48g Thank you!
سلام عليكم اخي العزيز اذا كان يوجد في الماء الملكي رصاص كيف التخلص منهو
H2SO4
@@OwlTech333 اخي العزيز ألم افهم
ما برای کار کردن به چه صورت بفهمیم که فلز ما رادیوم هست ممنون میشم
Sir after is black color
What do you mean?
@@OwlTech333 sir when you finish litle be more late paladio is lite be more dark
Black paladio l thinkso l gotte sir,
16 👍👍👍👍👍👍👍👍👍👍👍👍👍👍👍👍
Спасибо!
Hello, good evening, my name is Diego, I'm from Brazil. do you have email so i can send some questions ?? for example: I have an ammoniacal solution containing palladium .... I added hcl and yellow pd salt precipitated .... IF I TAKE THAT YELLOW SALT AND ADD FORMIC ACID AND THEN GO PUT IN SODIUM HYDROXIDE, WILL IT BE BLACK LIKE THIS ?? .....I WORK WITH RHODIUM, PALLADIUM, GOLD AND SILVER ....IT WILL BE A PLEASURE TO EXCHANGE INFORMATION. HUGS
Yes it should be exactly as this
Озвучка повний пізд**.
Дякую за відео
Това е завотско рафиниране така се рафинира в целият свят точно така го правя и аз
Bravo!
След амоняка го въстанивявам с солна при пеха 2
И накуя ты его плавил?? Не проще ДОРЕ получить отправить на завод за 5 % на афинаж?? Куда отработку деешь?? Соседям по даче сливаешь))
нет, не проще
@@OwlTech333 Лицензия есть на драги?
How much would you sell that little button for? Have you given thought to opening a store or do you have one already?
This one was sold the same day it was made. Unfortunately it went for 20% below spot price
@@OwlTech333 aww! HTe it when it gets away from us for cheaper than value! I remember when palladium was 10% what platinum was. It was like copper or maybe silver. Now platinum is palladium's junior league metal, like silver is gold's... anyways. Just curious.