how to calculate crystallinity from XRD data using OriginLab - 06
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- Опубликовано: 22 авг 2024
- Reference paper:
doi.org/10.108...
In this video, I have shown a simple approach to calculating the crystallinity of material from XRD data using OriginPro software and an Excel sheet. If you need any help or have any questions, then feel free to ask in the comment section below. For more videos, please subscribe to my channel. Thank you.
#NanoWorld
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Thanks a lot NanoWorld. This video helps me coz i got the reviewer's comment, it said to calculate the % of crystallinity. Thanks again.
me too and i am trying to calculate it, does it work with u using this software and method??
@@imandankar4807 yes, it worked.
Thank you very much please we need more video like this ,about how to use our data to get more info about our crystals, we need to hear your voice too)
Great job bro.
دەستت خۆش بێت
Your video was really very helpful, Thank you so much nanoworld. May ALLAH bless you immensely for spearding important knowledge. Aameen
thanks i get more information from your video lecture..
Thank you.
Thanks guys of the NanoWorld, this helped me a lot. Greetings from Brazil :)
Happy to hear that.
@@nanoworld6122
I just have one question. If I work with a very crystalline material, it will have many crystalline peaks. Should I calculate the area of all of them in the angular range? Because there are many :(
@@rauloliveira9579 Yes, If all crystalline peaks belongs to to your material then you must calculate area of all the peaks. As i did in this video.
@@nanoworld6122
I understand. In fact, when the worked material has many crystalline peaks, the work becomes larger. For these cases would Rietveld's method be better?
@@rauloliveira9579 Yes, Rietveld's refinement is an automatic and more reliable method as compare this manual method.
Thank you so much sir. Allah bless you always.
Thank you so much nanoworld. These videos are really helpful.
Thank you very much. This video helped me a lot. If possible please upload videos explaining (i) how to index XRD peaks of a crystal (ii) how to index SAED pattern
thank u so so so much for this amazing video. It really helped and is presented in the most perfect manner.. keep the good work going
Glad it helped!
sir you doing awesome job. please make video on reveilment method.
How do we know where to set the baseline?
Amazing, Thanks a lot...I have learned very important thing. Once again, Thank You So much
@NanoWorld
Thanks for the great job. My question 1, does overlap of area for near peaks affect the calculated crystallinity? Question 2 , does making a smooth graph and correcting baseline affect the calculated crystallinity?
For future reference, smoothing shouldn't affect the results much as long as not too much information is lost in the process, but baseline correction obviously affects results. Generally, having a baseline that's too high will reduce the crystallinity percentage.
Thank you so much for uploading this video🙏
thank you so much, this video is really helpful
the material was really useful,, Thanks alot
Thanks
Thank You so much. It was very beneficial to me.
My pleasure.
great job thnx very much. please could you tell me how i choose the constant according to the data
nicely done ❤
Thanks ever so much🙏
Thank you very much, it is helping me more, once again thank a lot
Thank you so much for sharing this calculation. It is really useful.
Perfect for lazy readers like me. Thank you!
😛
Thank you so much for your work... It will very helpful for me!
you are welcome
Should I adjust the baseline so that it touches some base-part of XRD graph?
Excellent work
Very useful video
Thank you so much. This video really helpful.
Thank you sir for this tutorial
thnx so much. could i know what is the benefit from calculating crystallinity of material
Kindly upload videos on Raman and PL fitting using Fityk
Thank you very much sir for this informative video...
Most welcome
thank you so much it is very much useful
Enjoy...
thank you very much
how to measure the baseline?
Thank you very much!!!
Do u have video how to calculate volume fraction from XRD ?
How to integrate from 10 to 90 to get the whole area? And how do you know that in thsi case - you have taken all the peaks ?
take all the area ...
can I do it, with raw data or I have to do some pre-step before do it?
because I'm facing baseline problem in my data, some values are fine but some peaks are coming below the baseline.
so please try to clear my doubt.
Please answer, cause ive got the same problem
Hi,
I have question about calculation crystalline index (CrI)
I've seen this ref of inorganic compounds, so with this method
1/ Could we use for polymer materials?
2/ Is this a relative method ?
3/ Do we have another method to check this method? (I mean calculate CrI by another method and compare with this method?
I hope I would receive you answer soon.
Thanks so much.
can you plz make video on how to determine rate constant of dye degradation on origin from lnC/Co vs time please please
i'll try.
I will be eternally grateful to you
what about the value of amorphous?
Thanks
@NanoWorld, now I can calculate % crystallinity easily coz of ur good instruction. But I would like to ask about which method is it based on? coz I need to write this calculation in Materials and Method section. May I know any reference to cite in paper. Thanks to again.
You may cite this article as a reference,
doi.org/10.1088/2053-1591/ab0aaf
What are the units of area?
do you have a research article were this equation was applied? I can not find an article where the equation was used
Can u please send me the xrd data for practice to plot multiple graph in origin
You can measured your samples and do it.
could you please suggest reference article on this medthod
At 3:45 minute, i cant select my peak. Kindly reply me, i sent a message on FB. Thanks
double click
Im very interested with this
Obrigado!!
I am not able to find peak analyser in my originpro. Please help.
Okay, How can I help you?
Thank you so much, can i connect with you please.
You can contact me through email. (Email address is available in the description of video)
What is a unit of measurement. Area of Crystalline Peaks؟؟؟
Area unit = counts x 2theta
how do you know what i want all the time😂
Helo, I’m having trouble with my graph. It has too many highest peak compare to the peak in your video. May I get your email so I can further discuss my problem with you? The data also reach up to 2000 in excel. I really need help since this is related to my fyp project. Please respond and help me :(
Hello Ms. Nadia, you can contact us at,
fascinatingNanoWorld@gmail.com
You can also reach us through our Facebook page.
Send me your data, I'll check it.
@@nanoworld6122 you r very hopfull . I hope y can help me for my data XRD
need to buy origin pro 2018, 2020 or anything :(. i cant' use with origin pro 8 crack
No need to buy, Originpro 9.5 is easily available with crack. You can download and install it.