If you use NH4NO3 it’s a lot easier to stir, you can also use a bigger excess of H2SO4 to make it easier to stir if KNO3 is all you have. Another option is to mix your acid and nitrate and chill it in the freezer until the sulfate/bisulfate crystalizes out and decant your mixed acid into another beaker.
@@wonkagameplay ever thought of using chatgpt to assist you with that? its really easy and basic stuff, just balanced equations and mole to gram conversions. You'll find the balanced equation if you watch Dug's ETN p1 and ETN p2 in youtube
I think if AN is used the temperature when is added to the Sulphuric acid won't increase unlike KNO3, cause AN has chilling properties when is mixed with water and S. Acid contains water
I did it like this: for 2.25 grams of erythritol, 6 ml of nitric acid 65%, 12 ml of sulfuric acid 98%. Erythritol is finely ground and added in small portions and mixed well, the temperature during nitration should not exceed 20 °C. After adding all the erythritol, the mixture will become quite thick, nitrate at room temperature no higher than 30 °C for another 30 minutes and then pour into water.
Xin chào bạn có biết điều chế amonitrat không,nếu biết thì bạn có thể chỉ tôi không? Trước đây tôi đã từng được bạn chỉ một số thứ và thành công.Tôi rất biết ơn về điều đó❤❤
@@matthorrocks6517 i already have nitric acid and i want to use it and also i give pure product and i want to make sure that i take safety precautions for nitric acid method
A chemist friend of mine made a small batch with AN but the ETN he got it doesn't detonate when he hits it with a hammer it just disappears but it burns when heated over aluminum foil
@@sanchezic I do a bicarbonate wash, where my etn is dissolved in minimal amount of acetone then dumping it in around 1 litre, 5 percent bicarbonate. But I’ve noticed many more people using urea instead of bicarbonate now, Is there a reason? I think I saw something mentioned is SM but sadly I lost the thread.
@Polkem1 look up the channel "dug", it's a guy Dugan Ashley, he has a nice ETN breakdown in a 2 part series. If your familiar with etn, skip to part 2 (which is the actual synthesis video). Sodium bicarb is used to surface neutralize but urea is used during recrystallization to absorb the remaining acid so it can't recontaminate the etn.
Brother just use the sulfuric and KNO3 to make nitric acid and then use the mixed acid method. All you need is a retort to start. Ive done both and mixed acids is worth the wait. Way better yields, better quality, no hotspots and you can actually stir it. Good job though 👍 😁
what a pain, what's the yield of etn you got? it'd be extremely useful to know with the unusual choice of KNO3, usually NH4NO3 would be used, but still curious
It make potassiumhydrogensulfate and HNO3. potassiumsulfat alone works only if you destill it at higher temperature 150C. But than there are lots of NOX inside your nitric acid the KHSO4 destillation yields the good one. Thats why Woolwich arsenal hat 1910 around 150 tons of sodiumhydrogensulfate per week as an waste product thats the sold as draincleaner or recover H2SO4 from it.(Historical note)
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If you use NH4NO3 it’s a lot easier to stir, you can also use a bigger excess of H2SO4 to make it easier to stir if KNO3 is all you have. Another option is to mix your acid and nitrate and chill it in the freezer until the sulfate/bisulfate crystalizes out and decant your mixed acid into another beaker.
If ammonium nitrate was used instead of potassium nitrate, how many grams would I need to add?
@@wonkagameplay there is some nh4no3 synthesis on yt look at it
@@wonkagameplay ever thought of using chatgpt to assist you with that? its really easy and basic stuff, just balanced equations and mole to gram conversions. You'll find the balanced equation if you watch Dug's ETN p1 and ETN p2 in youtube
I think if AN is used the temperature when is added to the Sulphuric acid won't increase unlike KNO3, cause AN has chilling properties when is mixed with water and S. Acid contains water
@@MarineCy it Will still increase almost as same as kno3 don’t say this, it’s dangerous, sulfuric acid only has 2% water in this case
I did it like this: for 2.25 grams of erythritol, 6 ml of nitric acid 65%, 12 ml of sulfuric acid 98%. Erythritol is finely ground and added in small portions and mixed well, the temperature during nitration should not exceed 20 °C. After adding all the erythritol, the mixture will become quite thick, nitrate at room temperature no higher than 30 °C for another 30 minutes and then pour into water.
Bro you gotta test it and show friction aswell as impact and fire interactions. nice job otherwise keep spreading the power brother.
You can use nitric acid instend of kno3
hno3 40-70% 30ml h2so4 80-98% 50ml Erythritol 17 gram
this ratio i got etn 15 gram
sản lượng thấp 17gr erythritol 17gr=20gr ETN
@@Dao9950 I use nitric not like kno3
Xin chào bạn có biết điều chế amonitrat không,nếu biết thì bạn có thể chỉ tôi không? Trước đây tôi đã từng được bạn chỉ một số thứ và thành công.Tôi rất biết ơn về điều đó❤❤
@@Sontay23 sử dụng amoniac và hno3 nếu không có điều kiện mua những thứ trên thì bạn có thể thử mua cano3 và nh4so4 tại cửa hàng phân bón
Can you make a video for nitric acid method
Sulfuric acid becomes nitric acid when you add the potassium nitrate.
@@matthorrocks6517 i already have nitric acid and i want to use it and also i give pure product and i want to make sure that i take safety precautions for nitric acid method
A chemist friend of mine made a small batch with AN but the ETN he got it doesn't detonate when he hits it with a hammer it just disappears but it burns when heated over aluminum foil
Make sure to wash your ETN many times, I do mine at Least twice, or 3 times. Still have 1g stored from 7 months ago, and it perfect conditions.
this is not enough, recrystallization in acetone with dissolution in water and urea is needed.
@@sanchezic I do a bicarbonate wash, where my etn is dissolved in minimal amount of acetone then dumping it in around 1 litre, 5 percent bicarbonate. But I’ve noticed many more people using urea instead of bicarbonate now, Is there a reason? I think I saw something mentioned is SM but sadly I lost the thread.
@Polkem1 look up the channel "dug", it's a guy Dugan Ashley, he has a nice ETN breakdown in a 2 part series.
If your familiar with etn, skip to part 2 (which is the actual synthesis video).
Sodium bicarb is used to surface neutralize but urea is used during recrystallization to absorb the remaining acid so it can't recontaminate the etn.
Brother just use the sulfuric and KNO3 to make nitric acid and then use the mixed acid method.
All you need is a retort to start.
Ive done both and mixed acids is worth the wait.
Way better yields, better quality, no hotspots and you can actually stir it.
Good job though 👍 😁
Your yield could be improved with smaller additions and stronger stirring.
at min 5 , do you clean the beaker with water or with sulfuric acid?
Pour into cold water
what a pain, what's the yield of etn you got? it'd be extremely useful to know with the unusual choice of KNO3, usually NH4NO3 would be used, but still curious
Where can you buy the spinner that stirs the powder to the liquids and how it works?
It's just a magnet that spins because the coil in which electricity flows generate magnetic field.
will you do PETN in the future
*Don't do this at home
What was the final yield?
Can u use erythritol with stevia or must the stevia be extracted out
You want it as pure as possible.
where is the potassium sulfate synthesized in the solution?
its a byproduct that is soluble so its in the crashed solution
Seems awfully easy to make... 😅
but what is there crystal or
but adding potassium nitrate won't make potassium sulfate?
yeah if you make h2so4 and kno3 it will make potatsium sulfate but i think we should make hno3 80-98% for etn
It make potassiumhydrogensulfate and HNO3. potassiumsulfat alone works only if you destill it at higher temperature 150C. But than there are lots of NOX inside your nitric acid the KHSO4 destillation yields the good one. Thats why Woolwich arsenal hat 1910 around 150 tons of sodiumhydrogensulfate per week as an waste product thats the sold as draincleaner or recover H2SO4 from it.(Historical note)
@@Preyhawk81 Okay
@@Preyhawk81 amazing grammar and spelling bro
What is ETN?
Do you use iphon 🤨
Erythritol tetranitrate (ETN)
Detonation velocity : 8200 m/s (best)
Shock/friction sensitiveness : Medium
but what do you do there what is
brother its not 125gr of sulfuric acid that you are using in hte video but 125mL, 125gr of sulfuric 98% would be 66mL
You are right, my friend, it was a typo
125ml sulfuric acid
can we use kclo3 instead of kno3
ETN = Erythritol Tetra NITRATE so you need a nitrate salt..
bludddd u have no business making etn if u ask if u can substitute chlorate for nitrate in a nitration reaction. learn chemisty b4 u make explosives.
Could this work using HCl?
no
try it and see what happens 😈😈