XRD X-ray diffraction worked example problem

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  • Опубликовано: 12 сен 2024
  • Worked example problem solution and tutorial for X-ray diffraction calculation. Materials science tutorial.

Комментарии • 69

  • @reinholdburchardt4581
    @reinholdburchardt4581 4 года назад +11

    Thank you very much, I spend so much time trying to understand our professor's crappy presentation. You are the first one to explain this stuff properly..

    • @TaylorSparks
      @TaylorSparks  4 года назад +1

      I'm so glad to hear it! Let me know if I can clarify other concepts. Also, like, subscribe, and share to help me grow my channel!

    • @waqasmuneer7951
      @waqasmuneer7951 4 года назад

      @@TaylorSparks Thank you professor for such a vivid explanation. I have one question which is confusing me. The maximum interplanar spacing will correspond to minimum value of h2 + k2+ l2? So it means it will be the plane having least integer sum?

    • @TaylorSparks
      @TaylorSparks  4 года назад

      @@waqasmuneer7951 Not necessarily!! That is only the case for the cubic system. In other systems the lattice parameters could make this untrue. For example, Consider tetragonal. The d spacing formula is 1/d^2=(h^2+k^2)/a^2+l^2/b^2. Here you see that depending on the values of a and b, it might not be right. For example, (001) will have a larger spacing than (100), even though these both have the same minimum value of h^2+k^2+l^2.

    • @bellarminefrancis147
      @bellarminefrancis147 Год назад +1

      ​@@TaylorSparks pppp

  • @iamitkumars
    @iamitkumars 5 лет назад +2

    Thank you so much for this tutorial. I was stuck for a long time until found this to rescue.
    Regards.

    • @iamitkumars
      @iamitkumars 5 лет назад

      Glad to see your response.
      Would this work same way for mixed metals? Let me know if I can reach out to you someway on this subject.

  • @srikarrepaka5023
    @srikarrepaka5023 4 года назад +1

    Thank you taylor for explaining me this
    Our professor is waste before you
    You're the best, nice explanation

  • @nilupulpiyumantha2108
    @nilupulpiyumantha2108 4 года назад +1

    Great explanation🔥 i'm from sri Lanka.Thank you

  • @satyanveshi36
    @satyanveshi36 5 лет назад +1

    explanation of which peak come first is good ! Thank You !!

  • @user-pg9dr2ni6j
    @user-pg9dr2ni6j 2 года назад +1

    Thank you so much. You save my life!!

  • @BBonBon
    @BBonBon 3 месяца назад +1

    Beautiful!

  • @mojong1098
    @mojong1098 3 года назад +1

    very very good, your presentation is clear and helpful, thank you!

  • @sionsterowzzz
    @sionsterowzzz 3 года назад +1

    one of those videos that save your ass before an assignment

    • @TaylorSparks
      @TaylorSparks  3 года назад

      I gotchu covered ;)

    • @SerweeFitness
      @SerweeFitness 3 года назад

      Oh my god, me too 😅.

    • @SerweeFitness
      @SerweeFitness 3 года назад

      @@TaylorSparks thanks bro, we love and appreciate you.

    • @TaylorSparks
      @TaylorSparks  3 года назад

      @@SerweeFitness ha! Love it. Do me a favor and check out our podcast "Materialism" on itunes and leave us a review!

  • @sophiehilsabeck5459
    @sophiehilsabeck5459 Год назад

    At 8:01 you said the lattice parameter was 0.329nm -- did you pick that because it was a3 or should we do some average of a1 a2 a3 to calculate atomic radius?

  • @zaynumar0
    @zaynumar0 5 лет назад +1

    !Taylor , thank you so much brother !!!!

  • @prabuddhamadhuranga5035
    @prabuddhamadhuranga5035 4 года назад +1

    Great explanation

  • @董育丞
    @董育丞 Год назад +1

    Thank you!

  • @zainebsiddiqui9392
    @zainebsiddiqui9392 4 года назад +1

    thank you so much. you cleared it all up.

  • @rajibdas1087
    @rajibdas1087 Год назад

    Superb explanation

  • @tejobhiru1092
    @tejobhiru1092 3 года назад

    thank you so much...this helped me a lot

  • @user-px3fp6ye9r
    @user-px3fp6ye9r 3 года назад +1

    thank you sir simply amazing!!!

  • @asst.prof.rohitnikam729
    @asst.prof.rohitnikam729 3 года назад

    Thanks..Is metal oxide have FCC or BCC structure.. if so far, how we calculate a from planes and spacing. If along with a how will you interpret for b and c in different crystal structure like tetragonal or orthorhomobic. I this you have calculated keeping in view for cubic system..kindly tell about any calculation to calculate R, a and b, volume of lattice which made easy for metal oxides like tin oxide. Please specify

  • @fauzansyauqi2815
    @fauzansyauqi2815 3 года назад +1

    sorry , but hoe you get the plane for FCC? I still wondering about it... please help

  • @ferozeahmadi8980
    @ferozeahmadi8980 4 года назад +1

    You are far better then my professor😍

  • @jamalkhatib7610
    @jamalkhatib7610 3 года назад

    Thank you for this information
    How to calculate Miller index in monoclinic system..like copper oxide

    • @TaylorSparks
      @TaylorSparks  3 года назад

      You can look up d spacing formula for monoclinic. It's pretty long.

  • @sheilaotuko4416
    @sheilaotuko4416 3 года назад +1

    May I inquire which tables you are referring to get the atomic radius

    • @TaylorSparks
      @TaylorSparks  3 года назад +1

      Here is the table I use. It is compiled from Shannon and Prewitt's classic paper www.mrl.ucsb.edu/~seshadri/Periodic/index.html

    • @sheilaotuko4416
      @sheilaotuko4416 3 года назад +1

      Thank you so much. You've been very helpful

  • @rahmpkorea
    @rahmpkorea 3 года назад

    tq for this! but where did u get the miller indices plane value? where is it came from?

    • @TaylorSparks
      @TaylorSparks  3 года назад +1

      can you be more specific?

    • @rahmpkorea
      @rahmpkorea 3 года назад +1

      @@TaylorSparks its ok! Got it already hehehehe tqsm for replying!

  • @charlottelim4964
    @charlottelim4964 2 года назад

    hi taylor, I was given a question which asked for interplanar spacing in FCC Aluminum expected slip systems, wouldnt it just be the calculation for d110? as [110] is the slip direction in FCC due to highest linear density.
    hope you can reply, thank you so much!

    • @TaylorSparks
      @TaylorSparks  2 года назад

      No. The slip direction is 110, but the slip plane is 111 so you need to calculate d_111

    • @charlottelim4964
      @charlottelim4964 2 года назад

      @@TaylorSparks dang.. however, from William D Callister's 7th Ed textbook chapter 3 Problem 3.57, it asked us to calculate interplanar spacing for Aluminum (110) set of planes. so how do we know when to do calculations for d110 or d111? would it be only when it's specified?

  • @Jehosafath
    @Jehosafath 2 года назад

    Prof how to approach if our structure is HCP or orthorhombic?

  • @faheemwani1996
    @faheemwani1996 2 года назад

    sir how to calculate lattice parameter of composite film with different concentrations of doping

  • @Eduardosbootss
    @Eduardosbootss 5 лет назад +1

    how do you know that the long diagonal of the cube covers 4 times the radius of the atom?

    • @TaylorSparks
      @TaylorSparks  5 лет назад +1

      This video covers that ;) ruclips.net/video/Tsj63DQ4yY0/видео.html
      It has to do with the type of structure, how the atoms close pack together and where they touch in the structure.

    • @Eduardosbootss
      @Eduardosbootss 5 лет назад

      Thank you, sir

  • @cy-ti8ln
    @cy-ti8ln 3 года назад

    how can we learn peak order from a xrd graph ? how can we trust if no information about peak order about xrd graph ?

  • @niloybasu2569
    @niloybasu2569 4 года назад +1

    where do you get the values of BCC AND fcc pLANES

    • @TaylorSparks
      @TaylorSparks  4 года назад

      at about 2 minutes in I go through how to generate BCC and FCC planes.

  • @firstkasihotang
    @firstkasihotang 3 года назад

    how did u figure out the first three peaks (miller indices) for FCC and for BCC?

    • @TaylorSparks
      @TaylorSparks  3 года назад

      I think that's exactly what I answer in this video. What exactly did you not understand? FCC versus BCC have different allowed hkl reflections so we went one by one and figured out which ones match the observed reflections.

    • @samkilgore9720
      @samkilgore9720 Год назад

      @@TaylorSparks I think he is confused how you drew the conclusion as to what Miller indices are to be used for FCC and BCC. They should already be known for ease of operation.

  • @stephenrose1902
    @stephenrose1902 5 лет назад +2

    I don't know how ,your plugging your numbers because you dont show it, I'm getting different results like .098357056 nm for the first value using 38.6., I used 38.6 degrees and I also, in case excel was treating 38.6 as radians did a conversion and my number are still way different. This is what I'm doing: .1542/(2sin(38.6)=dhkl =0.12358153785, I got it, you have to half the values because they are 2 theta,

    • @TaylorSparks
      @TaylorSparks  5 лет назад +1

      Hi Stephen. The problem is that 38.6 degrees is the value of TWO theta, not theta. So you need to divide theta by two in your sin function.

    • @stephenrose1902
      @stephenrose1902 5 лет назад +2

      @@TaylorSparks Thank you Mr. Sparks, I figured that out after I wrote to you, but I figured I'd leave the comment up in case someone else made the same error. I love your teaching style, thank you.

    • @TaylorSparks
      @TaylorSparks  5 лет назад

      @@stephenrose1902 thanks man!!

    • @tejobhiru1092
      @tejobhiru1092 3 года назад

      @@stephenrose1902 your comment really helped me.
      thanks for leaving it on..!

  • @SerweeFitness
    @SerweeFitness 3 года назад

    At 6:27 you started with part B in your problem and you used a table with atomic Radii and Crystal structure to determine the metal. I searched atomic Radii of more metals and there are Emperical Atomic Radii and Metallic Atomic Radii --->
    And you see with the table you provided at 6:27 I couldn't find accurate results as I found an element with a BCC structure and an atomic Radii of 0,1521nm and according to that table my best bet is Tantalum with a BCC structure and a atomic Radii of 0.1430nm, but I already used Tantalum in another example where I found the crystal structure BCC and an Atomic Radii of 0,1429nm.
    Source where I found the different types of atomic Radii --->
    en.m.wikipedia.org/wiki/Atomic_radii_of_the_elements_(data_page)

  • @ronaldivanwijaya6013
    @ronaldivanwijaya6013 4 года назад

    Do you have a reference for I learn this xrd?

    • @TaylorSparks
      @TaylorSparks  4 года назад

      I like this book www.amazon.com/Microstructural-Characterization-Materials-David-Brandon/dp/0470027851

    • @TaylorSparks
      @TaylorSparks  4 года назад

      another really great book is pubs.rsc.org/en/content/ebook/978-0-85404-231-9. It has many chapters in much greater detail

  • @imranasher1615
    @imranasher1615 5 лет назад

    Sir I tried this process but I didn't get ans
    I have 2 theta values of 44.3863 &98.3483

    • @TaylorSparks
      @TaylorSparks  5 лет назад

      I'm not sure that I understand. The two theta values are given in the problem. Are you trying to say that in your problem you are starting with different two theta values?

  • @Mr.G_Rattlesnake
    @Mr.G_Rattlesnake Год назад

    Cryptocurrency anyone?