Видео

How to prepare and run a sample for 60 MHz NMR. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to set up and run a vacuum distillation, using short-path distillation glassware and a portable vacuum pump. Although not included in the video, you could also insert a dry ice / acetone trap to maintain the integrity of the vacuum pump. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video starts with a review of how to pack, load, and run a chromatography column. It then shows how to use TLC to identify the location of colorless compounds. For a step-by-step video of column chromatography with colored compounds, see: ruclips.net/video/KGTZ3XBEfyc/видео.html This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to use column chromatography to purify a mixture of acetylferrocene and ferrocene. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to exclude oxygen and water from a reaction flask, by using inert atmospheric techniques. These include flame drying the flask, and adding reagents via dry syringes under a balloon of nitrogen gas. It is important to note that the focus of this video was on the techniques, and reactive materials were not actually used. Gloves should be worn while dispensing actual reactive ...

This video shows how to exclude oxygen from a reaction flask, by using inert atmospheric techniques. These include adding reagents via syringe under a balloon of nitrogen gas. Modifications for how to exclude water from a flask are shown in another video. ruclips.net/video/45dEG17rbwo/видео.html It is important to note that the focus of this video was on the techniques, and reactive materials w...

This video show how to prepare and run a sample for NMR on a 60 MHz Nanalysis benchtop spectrometer. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to use the program MestReNova to process a H-NMR spectrum of phenylethanol. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to clean an NMR tube with a suction apparatus. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to set up a reflux to heat an organic mixture. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to use a rotary evaporator to remove solvent from an organic mixture. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to take an IR of a solid using the ATR attachment. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to use a calibrated plastic pipette to deliver 1.5 mL of a bromine solution. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

This video shows how to test the bottom aqueous layer in a separatory funnel with a pipette and pH paper, to see if a bicarbonate wash was effective. This video can be used with the free downloadable laboratory textbook found at: organiclabtechniques.weebly.com/

IR of a Liquid

Drying Agents

Beilstein Test

Melting Point

Crystallization, Large Scale

Suction Filtration, Small Scale

Suction Filtration, Large Scale

Crystallization, Small Scale

Titration of an Acidic Solution

Fractional Distillation of Red Wine

Simple Distillation on Red Wine

Multiple Extractions

Single Extraction

Boiling Point Using ThieleTube

Running a GC