Recrystallization and Melting Point Analysis

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  • Опубликовано: 4 дек 2022
  • Now that we have covered some important separation techniques, let's take a look at a purification technique. Sometimes a chemical reaction will produce a solid, which can precipitate from solution. But these crystals typically contain impurities from solution that were trapped in the lattice as it formed. After we isolate these crystals, we can purify them via recrystallization. This is where we dissolve them in a particular hot solvent that will then retain any impurities before cooling it down such that it can crystallize again. We will also learn how to assess the purity of our recrystallized product using melting point analysis. This is neat stuff!
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Комментарии • 56

  • @nathanmermilliod3135
    @nathanmermilliod3135 Год назад +26

    Perfect video and explanation of concepts, and just in time for my students’ lab practical on recrystallization. Thanks Professor Dave!

    • @23100Battlefield
      @23100Battlefield Год назад

      I had my lab on this three weeks ago! Wish Dave had this video earlier, you really have labs late in the term, it's our exam period rn

  • @thomaseddyson362
    @thomaseddyson362 Год назад +9

    Thank you. I always appreciate the effort you go to with your videos. Well presented with just enough of the required ephemera.

  • @harrybrielmann189
    @harrybrielmann189 Год назад +1

    very complete! And I agree that trituration (forcing the solvent out by the addition of a less soluble solvent) often results in a less pure product.

  • @cancan1231ify
    @cancan1231ify Год назад +4

    Hey, I have friends and roommates that work for Thermo Fischer scientific. What a fun coincidence that they sponsored one of my favorite RUclipsrs.

  • @martinarenzi4744
    @martinarenzi4744 Год назад +2

    Thank you Prof Dave! As always so precise and clear

  • @hananehanane3860
    @hananehanane3860 Год назад +6

    I hope to see more techniques explanation in your channel. Thanks Prof Dave

  • @henna_nenna
    @henna_nenna 6 месяцев назад +1

    you are saving the life of every ochem college student thank you so much

  • @Dylan-cv7kj
    @Dylan-cv7kj Год назад +28

    Science is so cool

  • @eddielikesfish7114
    @eddielikesfish7114 Год назад +6

    i literally just learnt about this in chemistry lol. we are going to be making asprin with this method in january

  • @MSA_fansite
    @MSA_fansite Год назад +1

    I love you mr.dave you are really helping beyond imagination

  • @louisnemzer6801
    @louisnemzer6801 Год назад +1

    My favorite organic chemistry purification method!

  • @prixynealojado6998
    @prixynealojado6998 8 месяцев назад

    You're my hero, Professor Dave 🫶

  • @nicco-sixty
    @nicco-sixty Год назад +7

    Will you do more in-depth concepts in multivariable calculus, like the Jacobian matrix?

  • @vspqrv9784
    @vspqrv9784 3 месяца назад

    such a high quality video and explanation

  • @similosihlegqalisisa8211
    @similosihlegqalisisa8211 11 месяцев назад +1

    I'm subscribing now Prof❤❤❤

  • @TomasElizabeth
    @TomasElizabeth 2 месяца назад

    So super cool

  • @milviodeleon4421
    @milviodeleon4421 Год назад

    Wow comments on. Good job 👍

  • @Dont_insult_people
    @Dont_insult_people Год назад

    Fascinating

  • @ansammkh1681
    @ansammkh1681 Год назад

    thank you

  • @StephOnyia
    @StephOnyia 9 месяцев назад

    You are a pro 😮 Including the guy in the laboratory 😊

  • @rozana4470
    @rozana4470 Год назад +1

    When are the other videos coming cause i start OC lab this week😭

  • @gamingwithrksaver4868
    @gamingwithrksaver4868 Год назад

    We used to do these for derivative tests... and then match the m.p. to literature value to confirm the compound

  • @rassimsimou1594
    @rassimsimou1594 Год назад +1

    Good

  • @RevilHermes
    @RevilHermes Год назад +1

    I remember doing much simpler version with salt.

  • @missionsuccess6323
    @missionsuccess6323 10 месяцев назад

    . Synthesis of 2-Amino-4-(substituted-phenyl)-1, 3-thi-
    azole Derivatives

  • @TheCosmicGuy0111
    @TheCosmicGuy0111 Год назад

    Wowza

  • @enzoshii
    @enzoshii 8 месяцев назад

    Crystals did not form in our experiment. What could have gone wrong?

  • @WanderTheNomad
    @WanderTheNomad Год назад +1

    5:17 Why do we have to use the minimum amount of solvent? Is it just to avoid wasting it or something? Or is there another reason?

    • @keypo790
      @keypo790 Год назад

      Its because the experiments relies on Solubility Curve.

    • @user-qe8gy1zv2i
      @user-qe8gy1zv2i 11 месяцев назад

      its better to use the smallest amount of solvent to minimize the amount of material lost by retintion in the mother liqour

  • @krabre1848
    @krabre1848 Год назад +2

    hi

  • @chrisaltaawesome
    @chrisaltaawesome Год назад

    thank youuu

  • @Linda-hn3bh
    @Linda-hn3bh Год назад

    👍😌

  • @harrybrielmann189
    @harrybrielmann189 Год назад +1

    it's ok if the impurity is insoluble, just filter it out while hot.

  • @livingcodex9878
    @livingcodex9878 Год назад

    おはようございます

  • @-JA-
    @-JA- Год назад

    🙂👍

  • @judeboys6409
    @judeboys6409 Год назад +3

    This video reminds me of being a meth head in my 20s. Wouldn’t recommend it 😂. I used to “wash” it in acetone. To clean out impurities .. Have no clue what that was doing scientifically. But it sure made you higher 😅😮. Hey Dave. What would be the science of that lol ? You probably more an idea than I

  • @tiptop1681
    @tiptop1681 4 месяца назад

    Finally i can do this with my meth. Thanks

  • @worldsfinestsimp6421
    @worldsfinestsimp6421 Год назад

    TIGHT TIGHT TIGHT

  • @kevinxavier2986
    @kevinxavier2986 Год назад

    Komenke41

  • @desmond3828
    @desmond3828 Год назад

    immunology?!

  • @krabre1848
    @krabre1848 Год назад +1

    idk whats happening but cool

    • @krabre1848
      @krabre1848 Год назад

      omg i remember this in year 7

  • @KasaJiso
    @KasaJiso Год назад

    First comment, day to of “do more flat earth vids they blew up.”
    Sorry not first I was too long to write the comment :(

    • @Gxlto
      @Gxlto Год назад +4

      Sorry man I dont think he will. It's kind of dead at this point. I hope he does more creationism debunking

  • @DavidP089
    @DavidP089 Год назад

    2 million subs and your videos barely reach 10k views 🤔🤔🤔

  • @white_isnt_a_race2338
    @white_isnt_a_race2338 Год назад +1

    Educate me daddy