Hi, we tested the presence of palladium in the solution with tinus tin, the color turns first black then yellow and then orange, but we can not precipitate it using DMG, it is worth mentioning that after 4 hours of boiling the solution is still Too much metal powder remains in the container, DMG smells bad, can you help us identify the remaining metal or what is the way to contact you? Messengers or emails to send pictures
Congratulations for the video, the Pd is the only precious metal that combines, in acidic conditions, with DMG, it gives a very bulky and difficult precipitate to filter and wash properly. It is possible that after the Pd DMG calcination part of the Pd is oxidized but if you continue heating to more than 800 ° C that oxide decomposes again to a metallic state without the need for formic treatment. There can be a lot of loss of fines by dragging of PdO and Pd sponge during calcination. Regards
@@OwlTech333 The finally divided Pd oxidizes with relative ease and it is essential before leaching it to reduce it with formates, hydrazine, etc., because the PdO is not attacked even with aqua regia.
OwlTech How much in American dollars did you get? It looked like it was just under 2 grams right? Last question is, what was the purity of the palladium button? I hope to hear back from you, if you have time. I'm a first time viewer to your channel. I'm going to subscribe to help out. I love ewaste, its been a big passion of mine. I've learn alot about the ewaste collection from Ben. He's the best if you want to get serious about collecting the items you need like mlcc's.(Ben from Australia) GREAT GUY!!!
Why is it taking so long to luquify shoot my palladium somethimes depends on the purity I leave it will melt with a high heat lighter palladium supposed to melt quick but it may be dirty with pt
In my case - by adding DMG solution to palladium nitrate solution. The palladium nitrate solution was from treating palladium-silver dore alloy with nitric acid. The Pd-Ag dore I've got from cupellation of MLCCs.
@@OwlTech333 Last night I made my first gold extraction from CPU pins, using Aqua Regia Solution. I followed instructions, except to the part where I stirred the solution with metal and wooden rod. Besides I have put about 150 g of SMB and the reaction still the same. Could you plz help me with your experience.
Да тегилек блатной . Молодец 👍👍👍👍
nice work my brother
Hi, we tested the presence of palladium in the solution with tinus tin, the color turns first black then yellow and then orange, but we can not precipitate it using DMG, it is worth mentioning that after 4 hours of boiling the solution is still Too much metal powder remains in the container, DMG smells bad, can you help us identify the remaining metal or what is the way to contact you? Messengers or emails to send pictures
Добрый день,не подскажете,при плавке хлорид аммония,как флюс,улет пд уменьшит или нет?
Не знаю, не пробовал
Congratulations for the video, the Pd is the only precious metal that combines, in acidic conditions, with DMG, it gives a very bulky and difficult precipitate to filter and wash properly. It is possible that after the Pd DMG calcination part of the Pd is oxidized but if you continue heating to more than 800 ° C that oxide decomposes again to a metallic state without the need for formic treatment. There can be a lot of loss of fines by dragging of PdO and Pd sponge during calcination. Regards
Gustavo Fiora Thank you friend!
@@OwlTech333 The finally divided Pd oxidizes with relative ease and it is essential before leaching it to reduce it with formates, hydrazine, etc., because the PdO is not attacked even with aqua regia.
Бред
Потери от 20% не избежны
Да и фильтруется дмг замечательно 😂👍
I liked this, really good job i m working on it too.
Heya !
Thanks for sharing your work !
Will you use dmg for refining you button again or use another method ?
Always a pleasure to watch you !!!!
I sold this one as is because I needed the money, but I'll make a video with the recovery and refining process.
OwlTech How much in American dollars did you get?
It looked like it was just under 2 grams right?
Last question is, what was the purity of the palladium button?
I hope to hear back from you, if you have time. I'm a first time viewer to your channel. I'm going to subscribe to help out. I love ewaste, its been a big passion of mine. I've learn alot about the ewaste collection from Ben. He's the best if you want to get serious about collecting the items you need like mlcc's.(Ben from Australia) GREAT GUY!!!
@@shaneyork300 about $60 the purity is visible @11:41 91.22% the rest being silver. I'm familiar Ben's work and I've learned a lot from him too.
OwlTech
Thank you very much for responding!
That's GREAT with the purity and price!!!
Круто! Когда я осаждал палладий формиатом натрия, у меня получилось 92,6%, но был цинк, серебро, олово, цирконий, медь
Homer Simpson нет, с ним не работал :)
Good! Palladium is prity high this days!
😍😍😍
Hi Your formic acid is a few percent for boiling palladium ? Diluted acid formic or concentrated
Hello Friend! what acid did you use to dissolve palladium?
Nitric
Примерно потери при переплавки дмг а не растворение в царе не замерял?
Думаю если по чистить осадок в муравьиной и потом в азотной вы получили Pd 999° , а вы как думаете?
Привет! Хороший слиточек палладия получился!)) Не подскажешь где покупал горелку для плавки и за сколько? Лови лайкос!!!
Спасибо Олег! Это обычная китайская горелка кислород/пропан для холодильную технику. 15-20 EUR
dneprholod.com.ua/p85200241-gorelka-diametr-podsoedineniya.html
@@OwlTech333
Понял. Спасибо
Why is it taking so long to luquify shoot my palladium somethimes depends on the purity I leave it will melt with a high heat lighter palladium supposed to melt quick but it may be dirty with pt
Muito bom, parabéns 👏👏👏👏
Where can these sponges be found?
Are you guys using a modified B tank for the burning?
nope, just oxy propane
Awesome video. How to get DMG -Pd from?
In my case - by adding DMG solution to palladium nitrate solution. The palladium nitrate solution was from treating palladium-silver dore alloy with nitric acid. The Pd-Ag dore I've got from cupellation of MLCCs.
@@OwlTech333 Thank you 😊
@@OwlTech333 Last night I made my first gold extraction from CPU pins, using Aqua Regia Solution. I followed instructions, except to the part where I stirred the solution with metal and wooden rod. Besides I have put about 150 g of SMB and the reaction still the same.
Could you plz help me with your experience.
Автор? Возможно таким способом получить Pd 999°???
Да
To precipitate palladium from nitric acid with DMG, do you have to neutralize nitric acid or not?
I never did when precipitating with DMG
@@OwlTech333 OK, you don't have to neutralize the acid to precipitate with DMG, understood, thank you very much
Hi, bro!
Do you add dmg powder directly to palladium nitrate?
no, I'm dissolving the DMG powder in soda caustic solution
@@OwlTech333 Thank you, bro!. What percentage of caustic soda solution is used?
@@OwlTech333What is the role of caustic soda?
Do you have an application on your smartphone to check the purity of the paladio, or is it a different device that I have to buy?
different device called handheld XRF analyzer
@@OwlTech333 ok
Бред несъюшь
Awesome
👍Чотка!Вроде муравьиной раньше осаждал ты.Зачем мука эта с прокаливаньем?
легко осождает палладия из грязного раствора. серебо и платину не трогает
@@OwlTech333 в маточном растворе pt не было,оксим зеленит?
@@СергейТарх нет только Ag и Pd
@@OwlTech333 ясно,у меня при цементации цинком из азы, pd выпал серым с блеском цветом,через день частично осадок покраснел...Не пойму причины.
Есть потери при таком обжиге?
Конечно есть. Обжиг проводят в закрытом тигеле чтобы снизить потери но все равно они будут. Меньше но будут
Ну плюс еще это же на дмг когда визуально осадка много а на выходе очень мало. Плавим кучу а на выходе то что мы видим
Ну теперь то лутьшэ стало с переводом
Good job bro...😂
Thanks!
Nice..JOB 👍👍👍 salam dari indonesia yg berkat chanelmu banyak yg bisa proses palladium 🇮🇩😂
👍
any one here, succesfull using this way?
Show
Not bad easy 150$ for you that day
true :)
Antap
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