XRD Pattern Analysis Using Match!
HTML-код
- Опубликовано: 12 дек 2024
- #XRD
Basic use of the Match software (free trial version) for analyzing the XRD pattern of anatase TiO2. You may download the free trial version from the website www.crystalimpa...
Please don't forget to take part in the poll. Watch the video, click the card when it appears and cast your valuable vote.
**Well, if you're wishing to get the data entry file having the d-spacings, 2 theta values, and the corresponding Miller indices (hkl) of a particular material (specific ICDD file number) then please check out this video: • Exporting XRD Entry Fi... **
Hey! I am now making videos using the Samsung Galaxy S6 tab. It's highly recommended to use. If you are a grad student you can have this pocket-friendly one. You can use a cool keyboard alongside, which will facilitate ease of working.
Link of this tab in amazon.in: amzn.to/3Fr00B5
Keyboard for Galaxy S6: amzn.to/3Hxmx0Y
Pocket-friendly iPad: amzn.to/3Ficawa
Elements of X-Ray Diffraction
amzn.to/3nxJMAm
Here's the amazon link to my new Dell Inspiron 3501 laptop: amzn.to/3FilqjU
Facebook Page: / ayansarkaryoutube
Thanks! I could not find the hkl value too! And one more thing, be careful with the hkl values displayed in the datasheet, one value was wrong. But this free software worked. Thanks, man!
First of all, let me wish you a HAPPY INDEPENDENCE DAY of our beloved motherland.
Thanks for your interest in my video. I have found that sometimes, the (hkl) values of a particular sample are different in different JCPDS entry files. Moreover, you may also find that the ICDD specified (hkl) values of a particular sample is different from what the JCPDS file shows. That is why the entry file number must be explicitly mentioned while one analyses the XRD pattern. However, later, I made a video where I had shown how to get the (hkl) values for ZnO. You may watch that video. I am giving the URL of the video herein. ruclips.net/video/R3e1caJXkPs/видео.html
*Please also, do not forget to subscribe to my channel. It is my humble request.*
thnks for the video.
I want to know if there are two or three items in a sample , how to identify them using Match?
Hello! i would like to appreciate your effort, you did well.
may I know how do you know plane 101 of matched values. (at 5:49).
You'll find the (h k l) values corresponding to the d-spacing or 2 theta values in the data base, from there you can assign the peaks. Although, I could not show the (h k l) values in the video, sorry for that.
I think the following video will help you in this regard.
ruclips.net/video/R3e1caJXkPs/видео.html
What is mean TIO2 78% amount?
Its mean The XX sample is Tio2 ?
Or data( numbers ) of XX sample = data of TiO2 ?
sir your explanation about XRD data manipulation is very well.but you also explain that there are a lot of peaks regarding particular materials when how we identify that which peaks denotes Ti element or O2 atoms and why we take always 2theta angle during characterization.
First of all, I wish to thank you for interest in my video. As far as your question is concerned, it is quite obscure to me. You can not get XRD pattern for O2 molecule here. However, when you are analysing your XRD data, you should check the XRD pattern for your substrate and other probable compounds which might have been synthesised, along with your material under consideration. This type of comprehensive analysis is essential for reporting your work in a good journal. In this video, as I have told, my sample was TiO2 nanotubes, grown on the titanium substrate. Using this particular XRD analysis software, I have shown how easily the resultant pattern can be analysed. Match software has itself discarded the possibility of getting the rutile phase TiO2, reducing the time for extensive data analysis. As I had speculated the presence of XRD pattern of Ti metal, coming from the substrate underneath, in the resultant XRD pattern, I checked for that.
As far as the 2 theta angle is concerned, you may read this post. www.researchgate.net/post/In_XRD_why_is_2-theta_used_instead_of_theta
Thanks for video, how can i save the smoothed/corrected XRD profile raw data.
Thanks for your comment. As I was using a trial version so presently, I do not have the access to this software. However, I think this video ruclips.net/video/R3e1caJXkPs/видео.html may help you. Please subscribe to my channel.
My experimental data and simulated data have a minute difference. What should I do for it? I am working on MOFs
Try to refine, if possible.
what is I/IO means sir...
Urgent , how to get miler indices using match ?
Hi! There's one video. Hope, it'll be helpful.
ruclips.net/video/R3e1caJXkPs/видео.html
Please subscribe if it's helpful.
thnx alot for the video. do you have a MDI JADE 64 bit new version please
Sorry! I don't have that.
@@AyanSarkar1 it is ok thnx
Sir i'm using match software for barite samples and i'm getting barite and quartz peaks at same value how to differentiate it kindly give me your suggestion
Is quartz present in your sample? Is it the substrate? If not then you have no problem with quartz.
@@AyanSarkar1 sir i ddnt get your answer and yes quartz is also present in the sample and if both quartz and barite peak values are same then how we have to interpret.
@@siddhuhiremath9856 Okay! It happens for samples whose XRD peaks are positioned very near to each other. In those cases (if the samples are nano-sized), you can take the help of the SAED pattern analysis and lattice spacing calculations from the HRTEM micrographs.
I have a few XRD datas with ".opj". How can i convert ".opj" to ".mtd"? Help.
Sorry, I have no idea about it right now.
Open the .opj file with Origin software
Then Click the datasheet
Copy the data you want, and paste it in notepad
Save the notepad data file in .dat format
Using powdll software convert into whatever the format you want and you can use that file to analyse it in match software
how can I reuse match after the trial period is over?
I think that you have purchase the software then.
Can I know the phase if cubic or fcc
You have to check the corresponding ICDD data sheet.
Thanks it is interesting, How to export to Excell sheet
Please watch this video: ruclips.net/video/R3e1caJXkPs/видео.html
After you get the text file, you can open it using Excel. (Watch this video for guidance ruclips.net/video/Z5IfpooqXak/видео.html)
I'm having a problem with the software. When I try to run an analysis the following message shows up: "unable to read the Fullprof log file ('fplog.log')". I've already tried to reinstall the program, change the pathway and it did not work. I couldn't find a solution neither on the manual or the internet. Please, can anyone help me?
You may write to the company stating your problem.
Can you say the extension of your data file
Sorry! The license has expired.
Would you please tell me through the email for me.....I need to learn please
What's your question?
thank you
You're welcome.
Thanks !
You are welcome.
THANXS FOR THE VIDEO SIR
Thanks for your appreciation. Please subscribe.
thank u so muchh