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Hello dears, I am using XPERT high-score software to analyze the cement mix's XRD results. Although the major phases have emerged, I am having some issues. 1. Why do the main phases chosen from the pattern list not show up in the section on refinement control? 2. During double-clicking, one of the primary phases to view the details, there is no section on the structure and anisotropic displacement parameters. 3. Aside from these treatment options, how can I refine my graph to make it more readable? I would appreciate it in advance.

Thank you very much for your high quality content and dedication. Really hope your channel will be seen by many more people. I got solo-access to a xrd about a year ago and since then I'm more or less teaching myself with literature and webinars (to be honest, the whole reciprocal space, symmetry and rietveld - thematics are very challenging, but "simple" measurements and phase qualification is getting better). My high-score software version is quite old (2.2) and the refinement controls aren't like in your tutorials, I guess the database is a bit outdated, too. Your content is incredibly helpful and your slightly longer introduction-video got me hooked. I'm very interested and looking forward to your next video - series, already ordered the book you recommended. Wish you and Benjamin all the best.

great explanation, really helps to understand how it works

Hello! Nice video! So, how can I make a Vegard’s law XRD plot? What kind of software can make the quantification?

Thank you

Excellent must continue

me, a graphic designer: ah yes, this is incredibly relevant to me

I am impatiently waiting for more videos...! Thanks

Thank you for the wonderful effort you made on the expert score tutorial. I am using COD database compatible with Xpert highscore plus for Rietveld analysis. I continued with the tutorial until the step you change the phase asignments to pattern by CTRL+A and right clicking. After doing so, I did not find any numbers or phase names appearing on my graph.

I'm unable to fix the very low-intensity issues even during optimization (2 theta, omega, and Z). Can you please guide how to fix it?

how can we determine each peak is correspond to which planes???

More videos please...! please please

Hartmann Neck

Will You please provide me your email. I am facing some problems to fit some sample and I need your help

Thanks for video. How can I draw all the graphs obtained from HighScorePlus in OriginPro? Is there a way to get the data?

Perfect

Can you Please explain it for all no cubic

Thanks for your contribution. I have a few questions if you can help me. After matching all phases in a multiphase structure and adding CIF files, some peaks do not match after refinement. How can I fix this situation?

Hi I'm following your guidelines but in my data, no candidates found appears. can you tell me its solution?

Sir can we use Rietveld parameter in organic field

How to quantify the phases in cement (which is a complex material containing tricalcium silicates, dicalcium silicates, tricalcium aluminates, tetracalcium alumino-ferrites, and others?

Bit difficult to understand ur accent. Video is good though

If you have access to a workshop you could make vaccumholder, much better then tejp. Mikael Ottosson XRDLab- Uppsala University The Ångström Laboratory

Nice set of videos! Is in any of them explain how to correct for 2theta displacement using an internal standard (Al2O3, SiO2, ...)?

thank you for this great stuff.

Which software do you recommend for this?

can you share the excel template

Hi Michael, do you count with a configuration for capillary samples? If yes, what configuration and program are you using?

Hi. may i ask why my percentage does not appear?

hello, thank you for your explanation and video. For some samples, some people add internal standards in the powder. Why it is necessary?

How d= h2+k2+l2 i means is it any formula?

This is a really good video on XRD. Extemely underrated.

Thank you for this video , i find it very clear however i can not find the solver tolerance button in my Highscore Plus version ( 3.0d)

Why did you not include O and its atomic coordinates? What if I had 4e Wyckoff positions, should I enter 4 sets of coordinates? Thanks in advance!

Which can it be the best way to fill it with water solutions? In particular to avoid bubbles when you use a syringe.

This tube alignment method assumes that the incidence beam divergence slit and the detector's central pixel are almost perfectly aligned in one line with the goniometer's center. Are the correct and reproducable positions of the slit and detector guaranteed by manufacturer forever or they are adjusted by a user somehow before the tube alignment?

where i can find formula for calculating penetration depth? not in program, just formula, please

I am a postdoc. This was one of the best xrd lectures I’ve ever seen Great work

Thank you very much for the video. I'm a new user with Empyrean. Coudl you please explain why the omega changes with different samples (at 4'30'')?

Are these sample holders specific to the device used? For e.g we have rigaku Smartlab. I am not sure if it would be compatible with this

Thank you very much

Thank you for sharing this helpful video. I appreciate your time and effort.

Hello sir.. My sample is BaZrS3 I am not able to find this in the list what should I do then?

What version of highscore is it.? Some parameters that you show do not appear in the one I have, and I can´t find where to look at the version you have.

Great explanation! Thank you so much!

What is miller indices valye for 22 i followed your video for my calculations

I need your assistance regarding analyzing the data, can I get your email

Hello. Many thanks for such an instructive video. I wanted to know what is your software version?

how much minimum amount of sample required for XRD ?