OrganoLeptic
OrganoLeptic
  • Видео 4
  • Просмотров 473 936
Preparation of 4-nitrobromobenzene and 2,4-dinitrobromobenzene from bromobenzene
Today only!
Two for the price of one: 4-nitrobromobenzene and 2,4-dinitrobromobenzene.
+ allergic contact dermatitis if you watch in the next 5 minutes
But seriously!
2,4-Dinitrobromobenzene is a mutagen and skin irritant. Skin contact should be avoided by wearing gloves as some people possess a severe allergy to the compound (like me for example!), resulting in contact dermatitis of varying severity.
The procedure for the preparation of 4-nitrobromobenzene is based on:
www.chm.uri.edu/mmcgregor/chm226/nitration.pdf
RUclips videos on the synthesis of bromobenzene:
ruclips.net/video/QaC2yEegs5A/видео.html by chemx01
ruclips.net/video/WMVu-KSPsCg/видео.html by ReactionFactory
Preparation of 2,4-din...
Просмотров: 7 160

Видео

Synthesis of benzyl chloride by the free radical chlorination of toluene using TCCA
Просмотров 19 тыс.7 лет назад
Today I'll show you how to make benzyl chloride. This synthesis was loads of fun. I especially liked crying due to low-level exposure to the product during the filtrations. I hope I'll get the chance to use this product in one of my planned synthesis. If all goes well it will be quite a bitter experience :) Synthesis of benzyl chloride by nucleophilic substitution: - ruclips.net/video/lWFTYQ-x-...
Extracting paracetamol (acetaminophen) from tablets
Просмотров 439 тыс.7 лет назад
Today we isolate paracetamol (acetaminophen) from tablets using acetone. Interested in how I will use this product? Join me and find out. Other RUclips videos about extracting paracetamol from tablets: -ruclips.net/video/F40CXylcTlE/видео.html -ruclips.net/video/dENk7aTFflY/видео.html If you would like to help me make videos you can do that by supporting me via Patreon: www.patreon.com/OrganoLe...
Isopropyl chloride (2-chloropropane) from isopropyl alcohol, hydrochloric acid and calcium chloride
Просмотров 8 тыс.7 лет назад
Today we make isopropyl chloride also known as 2-chloropropane. I plan to use this in the future to synthesize a chemical that I believe has a sweet taste. But what will it be and how sweet will it taste compared to sucrose (table sugar)? Join me and find out. The synthesis of cyclohexyl chloride on which this procedure is based can be found at either of the links below: - archive.org/details/V...

Комментарии

  • @Shibnibby
    @Shibnibby 23 дня назад

    Dont boil cocodamol. The codeine burns. Use cold water extraction

  • @WillBeck-lf1tp
    @WillBeck-lf1tp 26 дней назад

    Yo my first time doing this I have 30/500 I’ve put 50 in a bottle 😂

  • @Tommybean7
    @Tommybean7 4 месяца назад

    Wow! This is brilliant! 👍

  • @gregoryroulin768
    @gregoryroulin768 5 месяцев назад

    DOI: 10.1002/slct.201801168 Look at this, they have yield from 76% with 8hour sunlight , and ratio equiv. 1:1 ..

    • @lrmackmcbride7498
      @lrmackmcbride7498 5 месяцев назад

      Nice also verified it works with a standard tungsten bulb.

    • @Rinkachikuzu_SVK
      @Rinkachikuzu_SVK 2 месяца назад

      hi, do you think it will work with NaDCCA as well?

  • @b3notafraid960
    @b3notafraid960 7 месяцев назад

    You should turn it into meth

  • @forcedriven9328
    @forcedriven9328 8 месяцев назад

    I just need drugs

  • @jimparsons6803
    @jimparsons6803 8 месяцев назад

    Interesting and thanks. Noticed in your list, you did not include Ferric Chloride, considering the ease of use, I found odd.

    • @lrmackmcbride7498
      @lrmackmcbride7498 5 месяцев назад

      That would promote ring chlorination rather than adding to the methyl group.

  • @امیرعبرانی-ل4خ
    @امیرعبرانی-ل4خ 8 месяцев назад

    یکی که ساخت مت امف را بلده از صفر تا صد به من یاد بده

  • @ABURAAD199
    @ABURAAD199 9 месяцев назад

    I can provide the ingredients but I don't know how to prepare😢

  • @benwalter6564
    @benwalter6564 10 месяцев назад

    U fuckin druggos🎉 😂

  • @mikaelbjornson2666
    @mikaelbjornson2666 11 месяцев назад

    Could you use an UV lamp for this reaction? Like the ones used for curing resin prints? Or are they too weak?

    • @alguiendesconocido7294
      @alguiendesconocido7294 8 месяцев назад

      Probably you need a halogen or mercury vapor lamp >300 watts, both produces sufficient UV light for do a free radical chlorination. Also remember that borosilicate glass can absorb most of the UV-B and UV-C light, but based on some papers and threads in forums that I see, is probably that UV-A is sufficient for the purpose (UV-A is not absorbed by borosilicate glass, at least not significantly). If you want an high yield synthesis maybe you need to consider to buy a Quartz flask (specially if your plan is do other synthesis where you use chlorine gas generators and you don't want to deal with large amounts of chlorine to fully chlorinate a molecule, what means that you need to neutralize the gases with larger amounts of sodium hydroxide). However I don't think it's very necessary in most of the cases.

  • @fredericdesalpes5824
    @fredericdesalpes5824 Год назад

    Very good explanations and practicing ... Fred/France

  • @ВикторПятница-н8с

    Гатить попа

  • @antejl7925
    @antejl7925 Год назад

    Great video but unless you have a use for the product all chlorinated aromatics are bad news.... avoid.

    • @lrmackmcbride7498
      @lrmackmcbride7498 5 месяцев назад

      Mix with sodium hydroxide and it will degrade to alcohols, ketones, aldehydes and carboxylic acids.

  • @bunkiey
    @bunkiey Год назад

    Prolly gettin some some uhhhhh… totally not hydros tmr… hope this works😮‍💨

  • @MitchelPie
    @MitchelPie Год назад

    How to extract caffeine and acetometaphin and leave the rest?

  • @staceymcdermott4954
    @staceymcdermott4954 Год назад

    How many livers are still functional since this video got uploaded

    • @miss_akame
      @miss_akame 5 месяцев назад

      Mine won't be soon 😂 jk but I mean we are in a rabbit hole now

  • @stupinjer21047
    @stupinjer21047 Год назад

    I love you bae

  • @midwestchem368
    @midwestchem368 Год назад

    Holy crap the comment section missed the point. This is gold! 🤣 Definitely needed this though. I'm guessing it's just not that soluble in much correct? I'm trying to obtain most of 200g of acetaminophen for a couple projects and to see what I can with it. Honestly I'm probably being lazy and just want to do it in 1 or 2 rounds of extraction.

  • @vaxdemic5944
    @vaxdemic5944 Год назад

    Is this what the song "Pushing P" is about?

  • @harithanayanajith6932
    @harithanayanajith6932 Год назад

    Will this method work for prednisolone tables?

  • @AlmondChocolateMilk
    @AlmondChocolateMilk Год назад

    nile red’s long lost cousin

  • @simekon80085
    @simekon80085 Год назад

    CWE-cold water extraction. Oldest trick in the book for every cough tablet enjoyer.

    • @Arkskii-gf03
      @Arkskii-gf03 19 дней назад

      How do you do that I can’t find information on how anywhere

    • @teresa8793
      @teresa8793 6 дней назад

      ​@@Arkskii-gf03good question

  • @williamlarue725
    @williamlarue725 Год назад

    So would the codine be at the top of bottom asking for a friend lol

    • @lagrangiankid378
      @lagrangiankid378 Год назад

      The codeine salt would remain in the filter if the acetone is anhydrous, otherwise it would just get dissolved in water and end up with the paracetamol.

  • @khalibbrodie1534
    @khalibbrodie1534 2 года назад

    how do you capture something but take the tylenol out

  • @genesisfootball1542
    @genesisfootball1542 2 года назад

    But isn’t codeine bad for you too? Or is it just the paracetamol that is harmful?

    • @jayjames5130
      @jayjames5130 Год назад

      Too much paracetamol is really bad for your liver

    • @genesisfootball1542
      @genesisfootball1542 Год назад

      @@jayjames5130 I know, but I’m asking if Codeine is bad for liver too

    • @jayjames5130
      @jayjames5130 Год назад

      @Genesis Football ok. I do take codeine every day and it by itself is ok.

    • @marsoblivi0n945
      @marsoblivi0n945 Год назад

      @@genesisfootball1542 codeine like all pain killers have there place with many benefits. It’s user error and lack of knowledge that makes them dangerous. Just like anything else.

  • @ironside6812
    @ironside6812 2 года назад

    why you use acetone ?

  • @nowtyguys965
    @nowtyguys965 2 года назад

    how to make crystalmeth

  • @adelinyoungmark1929
    @adelinyoungmark1929 2 года назад

    everyone here is trying to make illicit drugs while i just want some DDNP.

  • @jackjohnson4586
    @jackjohnson4586 2 года назад

    Wow, I wish I had known about this sooner! I previously made benzyl chloride in my home lab using a chlorine gas generator, and it worked but was a real pain in the ass due to needing to maintain a consistent flow of chlorine, plus making chlorine gas without a fume hood was anxiety inducing even though my apparatus had no leaks and was filtered through two scrubbers. This method seems much less complicated and significantly safer. Also gas masks are quite cheap, and I can confirm that benzyl chloride is a highly potent lacrimator

  • @huseyingogusov8700
    @huseyingogusov8700 2 года назад

    Salam Zehmet olmasa asitleri necə oldurmek olar deyerdiz

  • @TheJuris1986
    @TheJuris1986 2 года назад

    Does it work with codeine?

    • @TheJuris1986
      @TheJuris1986 2 года назад

      So undissolved will be codeine?

    • @lagrangiankid378
      @lagrangiankid378 Год назад

      Yes, if the pills contain a codeine salt (like codeine phosphate or codeine sulfate), and if the acetone does not contain any water (anhydrous acetone), otherwise is just gonna get dissolved with the paracetamol. You would still have to separate the codeine from the pill binders though. Also avoid boiling for too much or the codeine is gonna get decomposed by heat (75% of codeine is destroyed in 1 hour at 200 °C). If the desired product is the codeine a cold water extraction might be preferrable.

  • @douro20
    @douro20 2 года назад

    Blue-violet laser light should work as well for initiation.

  • @tyt0uoff146
    @tyt0uoff146 2 года назад

    Is.france known for easy access to drugs in the wolrd ?

  • @sashaboarkin1499
    @sashaboarkin1499 3 года назад

    Where I can bay many glass bottles ?)

  • @ashleydube1154
    @ashleydube1154 3 года назад

    This video makes no sense acetone is highly poisonous if ingested. So if you're trying to extract codiene from acetaminophen, you obviously can't use acetone it will most likely kill you or make you extremely sick!

  • @sammyd7857
    @sammyd7857 3 года назад

    TCCA is just a crap chlorination agent, that is why the low yield. Too many chlorines on one molecule

  • @shadowtheimpure
    @shadowtheimpure 3 года назад

    I found this video in my recommended today, probably because I watch a lot of NileRed and Extractions & ire videos. By the way, you have a new sub.

  • @ThaFuzzwood
    @ThaFuzzwood 3 года назад

    There is one chain termination missing, and that is where 2 benzyl radicals form 1,2-diphenylethane.

  • @maduabuchinnachor3569
    @maduabuchinnachor3569 3 года назад

    Get to side name of respectful and solutions llf

  • @sagesarabia5053
    @sagesarabia5053 3 года назад

    This is super complicated. Anyone know a more simpler process or video

    • @adelinyoungmark1929
      @adelinyoungmark1929 2 года назад

      this is like as simple as it gets. the thing you want dissolves in the chosen liquid, while not dissolving the stuff you dont want. then you take your liquid which has your dissolved stuff in it and get rid of the liquid, and now your left with the stuff you wanted.

  • @alish5417
    @alish5417 3 года назад

    paracetamol is insoluble in acetone nor in water

    • @lagrangiankid378
      @lagrangiankid378 Год назад

      Paracetamol is soluble in acetone and in hot water.

  • @Muhammadislahmedia
    @Muhammadislahmedia 3 года назад

    ruclips.net/video/PmtxQsfOV9c/видео.html

  • @ramongonzales8517
    @ramongonzales8517 3 года назад

    we all know why we here

  • @iminsideyourwalls9432
    @iminsideyourwalls9432 3 года назад

    does this work with pseudoephedrine/paracetamol

    • @ianskwid7948
      @ianskwid7948 3 года назад

      Little kid u don't know what ur talking about lmfao

    • @iminsideyourwalls9432
      @iminsideyourwalls9432 3 года назад

      @@ianskwid7948 having seen the kind of content you're posting on your channel and seeing your face,seems like I'm not the kid here,buddy.Go back and play your dumb ass video games. Why are you even in this video wtf.

    • @karebuskusa6301
      @karebuskusa6301 3 года назад

      @@iminsideyourwalls9432 lol got mad cause he said you looked a fool and made yourself look even more a fool. Is this really the hill you wanted to die on?

    • @adelinyoungmark1929
      @adelinyoungmark1929 2 года назад

      no, i dont think this process would work with pseudoephedrine, plus itd be cheaper to buy pseudoephedrine as a bulk chem rather than spending tons on the meds to extract from, although you do need a license IIRC to buy the stuff as its a precursor for some illicit drugs, but im sure you knew that.

    • @lagrangiankid378
      @lagrangiankid378 Год назад

      If the acetone is anhydrous the pseudoephedrine salt will remain with the pill binders in the filter. But just a little amount of water would dissolve the pseudoephedrine too, especially the hydrochloride salt (with a solubility of 10 mg/ml).

  • @nurarifin2473
    @nurarifin2473 3 года назад

    Pengen buat sabu

  • @flaplaya
    @flaplaya 3 года назад

    Wonder what came over before 34 C ?

  • @dishankxyz4489
    @dishankxyz4489 3 года назад

    Can you do a pseudoephedrine extraction from sudafed

  • @alishinawii3502
    @alishinawii3502 3 года назад

    Can chlorine gas be pumped into the reaction flask directly and how to know it's enough?

    • @jackjohnson4586
      @jackjohnson4586 2 года назад

      I know this is old, but you definitely can pump chlorine into the flask directly via a chlorine generator made from TCCA and HCl. However, you better make damned sure there are no leaks or you'll have chlorine gas flowing out of the apparatus

  • @filmpilihankerenjalancerit4695
    @filmpilihankerenjalancerit4695 3 года назад

    Plis extract Ephedrin tablet