Platinum Laboratory Services
Platinum Laboratory Services
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Scientific glass blowing. Making a Liebig Condenser Tutorial.
A Liebig condenser is a very common piece of equipment for laboratories. I'll show how they are made. They are a good beginners piece of scientific glassware to attempt.
Просмотров: 3 514

Видео

Healing a crack
Просмотров 19 тыс.4 года назад
This is another video for beginners learning to work with glass. I'm demonstrating how you can heal small cracks in glassware and how to visualise the stress that occurs when glass has been heated up to it's melting point.
Glassblowing with a Bunsen Burner
Просмотров 5 тыс.4 года назад
For those who have wanted to get started with forming glass but don't have any special equipment, this little project of making a sealed ampoule is a good place to start. All you'll need is a piece of soft glass tubing of around 5mm diameter, a Bunsen burner and something to make a small jet of air attached to a blowhose. A pair of tweezers and a burnt piece of wood as a forming tool can come i...
Repairing an Apix tube base
Просмотров 2564 года назад
I often get requests to see how a repair is done, this video shows the steps involved in getting a base that has broken off, repaired and looking as good as I can make it.
Base repair flaring
Просмотров 1844 года назад
In this video I've used a different filter and you can see more of the glass being worked.
Making a Schlenk manifold.
Просмотров 1,2 тыс.4 года назад
This is my technique for making a dual bank manifold for air free work. Otherwise known as a Schlenk line, these manifolds are fitted with taps that allow a transfer of vacuum or in inert gas to a flask and it's air sensitive contents. This manifold is using the double oblique style of taps that switch the outlet to one or the other line of the manifold with a quick 180 degree turn of the tap. ...

Комментарии

  • @DYIIdeas
    @DYIIdeas 19 дней назад

    the crack in the graduated cilinder ran away a little bit but i managed to weld all the crack, using a mini butane torch and a gas cooking stove (without the cap on).

  • @mehdimehdi7290
    @mehdimehdi7290 23 дня назад

    I just had my glass blower make a liebig condenser for me. I ordered him to use a 13 mm diameter tube with 1.5 mm thickness as vapor tube. Now I'm worried 10 mm diameter as vapor path would be too narrow. Will you please shed light on this?

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 23 дня назад

      It really depends on what you are distilling and how fast you want to do it. A Liebig isn't great for low boiling substances like methylene chloride, diethyl ether and the likes. But substances like ethanol and water and higher boiling points, condense reasonably fast, and a Liebig does a pretty good job. So a slight restriction of the bore will lower the surface area a bit and slow down the rate at which you can collect the distillate. Variables like coolant temperature are going to make a difference, and so is the enthalpy of vaporisation of the distillate, so it's hard to say whether this small change is worth worrying about without knowing all the detail. Give it a go and if it's not condensing fast enough, remove some heat from the boiling flask and just go a bit slower is the best answer.

  • @paulvawter8205
    @paulvawter8205 Месяц назад

    Okay but how do you make sure it cools down both evenly and slowly? That’s the much harder part.., even if you repair it when it’s hot… it’s just going to crack again if you just take the entire thing out of the flame and into room temperature as that’s way too rapid and will just make it worse so… I feel like this is not really even quite half of a realistic process

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 Месяц назад

      Thanks for the question, it's a good one. Breaks occurring from large temperature changes are indeed a problem, but whole video is about spreading the heat over the entire piece using a bunsen flame and why it matters. A bunsen flame isn't too hot, and so to cool down from that temperature is not a problem for borosilicate glass. The temperature difference between the flame from an oxy torch and the temperature of glass in the bunsen flame isn't as wide as if the piece was at room temperature and so the stress is also going to be as bad either. In fact, cooling the piece down from the bunsen after the repair showed no stress at all with the polariscope. I demonstrated that this is a realistic approach to small repairs. Larger repairs with thicker wall glass and joins going through the wall cause more issues, and more care and specific pre-heating regimes are needed. And even then, with all the skill you have as a professional glassblower, it can still crack on you. An annealing kiln is absolutely necessary to take out residual stress after a complex repair. But if you come to understand how spreading heat over a larger area than just the point of the crack or repair work will prevent cracking , then you will progress your glass blowing skills and become more confident tackling more complex work. I hope that's what these videos are about.

  • @homieflores141
    @homieflores141 Месяц назад

    Can I make a meth pipe like this 😂

  • @monikasaringer1152
    @monikasaringer1152 3 месяца назад

    Didn't know about the polariscope, thanks for that, ive used although not as hot & will take longer my gas stove element or just a gas lighter depending on the repair & glass thickness

  • @lautaromorales2903
    @lautaromorales2903 3 месяца назад

    Excelent video! last month i healed a cracked test tube (to practice with something) and broken graduated cilinder with a huuge crack that i managed to rescue for use in my home. the crack in the graduated cilinder ran away a little bit but i managed to weld all the crack, using a mini butane torch and a gas cooking stove (without the cap on).

    • @m_chandler_72
      @m_chandler_72 3 месяца назад

      I'm happy to hear you gained the confidence to give it a go. And even got a win from it. I'm going to try and put more content up for beginners soon. Any suggestions for new videos are always welcome. Thanks for commenting.

  • @MAGATRON-DESTROY
    @MAGATRON-DESTROY 4 месяца назад

    Pretty ingenious!

  • @MAGATRON-DESTROY
    @MAGATRON-DESTROY 4 месяца назад

    Is that borosilicate you are using?

  • @BLove-dx7pd
    @BLove-dx7pd 5 месяцев назад

    Hey mate im new to this but could i use a candle and torch to do this method if i dont have the neat flame thing u have

    • @m_chandler_72
      @m_chandler_72 5 месяцев назад

      I don't think there'd be enough heat in a candle flame. Give it a go and let us know how you got on. Sometimes suck it and see is the best way to learn.

  • @jswp5
    @jswp5 5 месяцев назад

    Hey, idk if you're still checking comments, but if you are, what's that torch you're using alongside the bunsen burner? I've got a cracked glass I need to heal, and this is the only video tutorial I could find

    • @m_chandler_72
      @m_chandler_72 5 месяцев назад

      Thanks for watching and reaching out. I've got a small hand torch which runs off propane and oxygen, they are used by jewellers and some other crafts. But a small brazing torch for plumbing can also be used, so long as it runs on oxy/fuel and has a small enough tip.

    • @jbriant29
      @jbriant29 3 месяца назад

      "Smith mini-torch" he said in the video.

  • @billyngarotata4427
    @billyngarotata4427 5 месяцев назад

    Crackheads be running to there dealer watching this😂Thanks for the hack

  • @n00bslayherttv92
    @n00bslayherttv92 6 месяцев назад

    I feel like if you reedited this video and posted again it would take off some more - was just a wee long, albeit very informative

    • @m_chandler_72
      @m_chandler_72 5 месяцев назад

      Hi and thanks for commenting. It's a fair point you make. I think I'm in the zone that many early content creators get into. We just want to get the info out there, and getting a video together is hard, editing is also really time consuming and has a learning curve all of it's own. So I'll own my early cringey work with it's unpolished edges, and I'll strive to get better with future projects. If there's some techniques or glassblowing details that need a deeper dive that others might have missed, let me know.

  • @Jan_Seidel
    @Jan_Seidel Год назад

    13:30 did the glass crack that clean just because of a very focussed flame? I have never seen that before.

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 11 месяцев назад

      Flame cracking. Yes it's my preferred technique for cutting glass tubing. Make a score on the glass using carbide. Ive found router blades or boring bars for metal lathes a great tool for this job. Then turn the glass so the score is facing you with the tube in both hands. Come from under the flame, a small sharp flame, and touch the glass ahead of the score that is away from you with the flame that is very close to the tip of the torch. Rotate the glass so the flame just touching the glass creeps towards the scoreline. With the right amount of heat and the right speed of rotation it will crack reliably around the glass. Cold glass makes a less precise cut, the glass is brittle and the crack wants to find the path of least resistance. So using the warm air above the flame you rotate the glass where you want the crack to go. It should be not much warmer than body temp. Give the glass a few seconds to allow the heat to penetrate to the inside of the glass. Then use the technique described to cut the tube. Practise practice practise.

  • @joshwhite9954
    @joshwhite9954 Год назад

    What kind of Bunsen burner is thst

  • @Kingfarter
    @Kingfarter Год назад

    What's this music playing? Thanks for the video

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 Год назад

      I think it's David Moufang. Otherwise known as Move D. It's probably this recording: ruclips.net/video/ILDuFIjDfLs/видео.html

  • @FunFunFunFun963
    @FunFunFunFun963 Год назад

    how are conections make?

  • @PneumaticsAreCool
    @PneumaticsAreCool Год назад

    I would absolutely love to be able to do this type of work.

  • @Bretaxy
    @Bretaxy Год назад

    Gloves?

  • @pharmdiesel
    @pharmdiesel 2 года назад

    Very good! Definately a skill worth learning; thank you!

  • @souljaboy2443
    @souljaboy2443 2 года назад

    Does this run solely on propane?

    • @m_chandler_72
      @m_chandler_72 2 года назад

      The bunsen says natural gas on it's base, but I run it on propane and it's fine.

    • @souljaboy2443
      @souljaboy2443 2 года назад

      Thank you 🙏🏼

    • @MAGATRON-DESTROY
      @MAGATRON-DESTROY 4 месяца назад

      Fuel gas and air through the venturi effect

  • @stephenlepore4476
    @stephenlepore4476 2 года назад

    nice set up man!i love your fixture. thanks for the video!

  • @cdog252
    @cdog252 2 года назад

    Plastic double oblique taps feel like a false economy on a Schlenk line.

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 2 года назад

      Glass taps seal better that's for sure. But they are prone to getting stuck. Researchers and students can often break a tap trying to get it free. So there are quite a few people who order the PTFE taps for practical reasons.

  • @SummersSnowVideos
    @SummersSnowVideos 3 года назад

    Hey mark, i noticed at 1:14 - 1:18 you specifically heat up the underneath of both tubes. Is this general heating, or is there something more to it? Specific stress occurs opposite the hole? i don't know why i noticed, but it seemed deliberate enough to pop the question into my mind. From Michael, the one Aussie over here in Germany learning the trade.

  • @nameyourchannel5181
    @nameyourchannel5181 3 года назад

    Great demo. Thank you. Quick question: for the ring seal joining the water jacket shell to the inner tube, did I see some initial sucking before you blew? At around 16:43?

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 3 года назад

      Well spotted, I did suck and blow a few times, small in and out puff and suck. It helps form the shape of the internal seal which I go on to explain is critical to prevent it cracking. Although I just realised the upload chopped the bottom off the illustration I did as an explanation.

    • @nameyourchannel5181
      @nameyourchannel5181 3 года назад

      @@platinumlaboratoryservices8176 Makes perfect sense. Thank you. The important bits of your illustration were pretty clear. Very impressed by how uncluttered your work area is and noticed you put away every tool after each use (looks like to dedicated spots). One surprise was how you used the flame to detach the cold seal. Will have to give that a try instead of knocking it off.

  • @machine2000ify
    @machine2000ify 3 года назад

    Great technique.

  • @tersecleric2
    @tersecleric2 4 года назад

    Really fascinating stuff. I assume the pipe in your mouth controls the "strength" or temperature of the blowtorch?

    • @veandreas
      @veandreas 3 года назад

      It's a blowhose, to give pressure inside the glass tubes, in this case to blow a hole in the tube as you can see at minute 1:05.

  • @arkomausa
    @arkomausa 4 года назад

    That was pretty damn cool. Arkoma

  • @Ubya_
    @Ubya_ 4 года назад

    good video! another way to make a polariscope (in case one doesn't have a big sheet of polarizing filter laying around) is to just use an lcd monitor showing a white image. what i do is rotating the small piece of polarizing filter near my eye (like the piece you placed over the camera in the video) until the white turns black (or in my case dark blue), if you then place the glass piece between the monitor and your filter and there's any stress in the glass, you will see bright white spots or bands

    • @platinumlaboratoryservices8176
      @platinumlaboratoryservices8176 4 года назад

      Very True! The monitor does work, the stress will show as black and white bands unless you place a sheet of something like clear polycarbonate in front of the monitor. Thanks for your reply.

  • @bdy0523
    @bdy0523 4 года назад

    awesome!