- Видео 18
- Просмотров 68 836
Ben Britton
Канада
Добавлен 1 сен 2013
ICOTOM'19 - 2021
Research talk for the ICOTOM'19 Conference held virtually: "A data science approach for characterisation of fine scale feature using correlative electron backscatter diffraction and energy dispersive spectroscopy"
Tom McAuliffe1, Alex Foden1, Chris Bilsland1, Ruth Birch1, Thibaut Dessolier1, Dafni Daskalaki-Moutanou1, David Dye1, 〇Thomas Ben Britton1 (1.Imperial College London)
The associated papers are published, and can be found as preprints here:
Many precipitates in superalloys: arxiv.org/abs/2009.00948
Gamma and gamma' separation: arxiv.org/abs/2005.10581
Introduction to PCA with EBSD and EDS: arxiv.org/abs/1908.04084
Tom McAuliffe1, Alex Foden1, Chris Bilsland1, Ruth Birch1, Thibaut Dessolier1, Dafni Daskalaki-Moutanou1, David Dye1, 〇Thomas Ben Britton1 (1.Imperial College London)
The associated papers are published, and can be found as preprints here:
Many precipitates in superalloys: arxiv.org/abs/2009.00948
Gamma and gamma' separation: arxiv.org/abs/2005.10581
Introduction to PCA with EBSD and EDS: arxiv.org/abs/1908.04084
Просмотров: 613
Видео
Introduction to EBSD: Section 2 - EBSD & Crystal Orientations (ft. basic crystallography)
Просмотров 10 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 2 - EBSD & Crystal Orientations (ft. basic crystallography)
Introduction to EBSD: Section 4 - Pattern indexing
Просмотров 3,6 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 4 - Pattern indexing
Introduction to EBSD: Section 3 - Pattern formation and capture
Просмотров 6 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 3 - Pattern formation and capture
Introduction to EBSD: Section 1 - What can EBSD tell you?
Просмотров 15 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 1 - What can EBSD tell you?
Introduction to EBSD: Section 5 - Validation of Orientation Convention & Coordinate Systems
Просмотров 2,4 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 5 - Validation of Orientation Convention & Coordinate Systems
Introduction to EBSD: Section 8 - Some Future Directions
Просмотров 1,3 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 8 - Some Future Directions
Introduction to EBSD: Section 6 - EBSD Data Analysis
Просмотров 6 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 6 - EBSD Data Analysis
Introduction to EBSD: Introduction
Просмотров 3,2 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk The slide deck can be found here: drive.google.com/file/d/1_ifgAadOCVADSe_vI1UZ7-gNVkZKw6IB/view (This is slightly updated as compared to the videos, as I fix mistakes as I see them/or am told about them)
Introduction to EBSD: Section 7 - Conducting an EBSD experiment
Просмотров 1,7 тыс.3 года назад
Introduction to Electron Backscatter Diffraction (c) Dr Ben Britton, b.britton@imperial.ac.uk Section 7 - Conducting an EBSD experiment
Introduction to Focussed Ion Beams (for microscopy)
Просмотров 1,6 тыс.4 года назад
Introduction to Focussed Ion Beams Video by Dr Ben Britton, Imperial College London. For the associated slides - please visit www.expmicromech.com/techniques
Introduction to Energy Dispersive X-Ray Spectroscopy (EDX/EDS)
Просмотров 9 тыс.4 года назад
Introduction to Energy Dispersive X-Ray Spectroscopy (EDX/EDS) Video by Dr Ben Britton, Imperial College London. For the associated slides - please visit www.expmicromech.com/techniques
Introduction to Scanning Electron Microscopy
Просмотров 6 тыс.4 года назад
Introduction to Scanning Electron Microscopy Video by Dr Ben Britton, Imperial College London. For the associated slides - please visit www.expmicromech.com/techniques
Message for LGBT assembly - Dr Ben Britton
Просмотров 5614 года назад
This is a short video for @bristol_teacher to share with pupils about me as a member of the LGBT and STEM communities
Stable crack growth at the micron lengthscale
Просмотров 3637 лет назад
Stable crack growth at the micron lengthscale
love you
🥳thank you
Thank you so much Dr. Britton, it is really helpful!
Thank you for your video. I would like to ask, is the optical path construction of EDXRF similar to that of EDS? What should be paid attention to when constructing the optical path of EDXRF? What are the measurement standards? For example, the angle between the detector and the X-ray tube, and the distance between the detector, the X-ray tube and the sample.
Thank you for your video. I would like to ask, is the optical path construction of EDXRF similar to that of EDS? What should be paid attention to when constructing the optical path of EDXRF? What are the measurement standards? For example, the angle between the detector and the X-ray tube, and the distance between the detector, the X-ray tube and the sample.
@@jianchaosongapologies I am not familiar with the XRF family of techniques
Thank you Dr. Ben for this wonderful introduction to EBSD series!!!
Very glad you found it helpful
Thank you doctor.Great.please make a video about how we can determine and guess phases with xrd result and eds result without using xpert highscore lonely.?
Thanks for the comment. I do not use those pieces of software, so I am unable to assist with this request.
Too bad explanation. Thank you for being so terrible.
hi thanks for such an informative video, can you provide any source of reference for EDS data particularly for microplastics?
I am afraid that I do not work in this area, so I am not up to date with how EDS could be used to understand microplastics.
Dear Dr. Britton, Thank you a lot for these videos. I am just starting with EBSD and I have some probably trivial questions. Concerning the first part of this video, when using multiple distinct reference directions most grains change their colour. This means that a certain grain will have one crystallographic direction more or less aligned with respect to that specific sample direction. By switching the reference, the colour changes, meaning that in that grain some other cryst. direction is now preferentially aligned with that specimen direction, right? Is three-dimensionality included in this? I mean, if the diffracted signal comes from a specimen region which in the c-direction inglobes more than one grain, what can I expect the orientation of that grain in the a-b plane to be? Thanks for your attention. M.B.
Hi - thanks for the feedback, and for the queries. The IPF map colour is just a representation of the orientation, and how the colour changes with a choice of reference axis depends on the symmetry of the unit cell and the texture of the material. Imagine a cubic crystal, if you have it aligned with [100] (red) along X, and [010] (red) along Y - it will not change color when you switch between these axes (note it will also be red when you use a Z reference axis). If it is rotated 45 about X, then it will be red still when X is the reference axis is used, and now a different color when Y/Z is used.
Hi Dr Britton, from your paper and this video, i take that the Kikuchi maps obtained should be overlayed on a SEM image only when we have rotated it 180. I have a 100 single crystal and am trying to find {100}<100> direction. Also, for the kikuchi maps, should i overlay it directly or should i have to multiply by a factor( for PCx or PCy)?
Hi - thanks for reaching out. Unfortunately I don't know what you are trying to do, and neither of these solutions sound right/reasoned of themselves.
Hi Ben, thanks again for the great lecture series. In a standard FIB-SEM arrangement the EDX detector cannot be on a horizontal port of the SEM, meaning that tilting the sample will introduce shadowing from the detector. Do you think it's still possible to record EDS spectra at 70° tilt in such a configuration and measure EBSD and EDX and the same location? And what's your opinion on combined 3D-EDX and EBSD (combined with Ga or Xe-FIB)?
We have done EDX + EBSD. It requires a bit of work due to the interaction volume (more than shadowing). We are about to do 3D pFIB EBSD+EDX...
Hi Ben, thanks for the nice introduction to EBSD and basic crystallography :-) very helpful and well explained!
Thanks for the kind feedback!
This series is really helpful!! Thanks Doc!
That's super kind, thank you for the feedback
thanks very much Dr
Glad you found these useful/interesting!
thank you for this series, it has been effectively illuminating.
Thanks for the feedback and watching the series!
dislocations movement
👍,
🇬🇧🇺🇸
Thanks very much! It was a great overview!
Thanks for watching!
Nice video Ben. Could I ask about a K shell (1s2 say) electron being promoted to a higher energy L shell (2s2 say). How could that happen as the 2S2 level will be completely filled. Is it more correct to say the K shell electron will leave the atom and an electron from the L shell will take its place. Then an electron from an M shell will fill the vacancy left by the L shell electron i.e. there is a cascade? Thanks
Err - not sure that we would label which transition occurs this specifically in EDX - these effects are seen when we model the probability of each transition, which guides peak heights
Is that a knitted/crocheted EBSD pattern blanket behind you?!
Yep - it is - made by Dr Vivian Tong
Nice 👍
Thanks for the feedback
Nice 👍
thank you thank you thank you. This is great!!! there are not as much info for ebsd on the internet as other electron microscopy techniques. Would love to see more about sem's and also it would be great to give so bibliography for us that start to get into the subject... Please keep it up!
Thanks for the feedback. We wrote a review of EBSD that could get you started (I cite it in the slides, "strains planes and EBSD in materials science"). And if you look at my youtube videos there is a recording of a SEM introduction lecture too (but I need to work on it again for a serialised version).
Awwm
Thanks for the great content. would you please help me with the concept of TD, RD, ND, and how to determine them on a specimen? or if there is any related content that I have missed among your vids I appreciate it if you let me know.
Hey - thanks for viewing the video. There is a specific video where we explore the definition of the axis system for the instrument: ruclips.net/video/K5TOB99oCq4/видео.html This is also explored in a paper: www.sciencedirect.com/science/article/pii/S1044580316300924 RD, TD, and ND are three names used to define axes with respect to a rolled plate/sheet - with RD = rolling direction, TD = transverse direction, and ND = normal direction. These should be defined with respect to the X-Y-Z (right hand set) used to index the diffraction pattern.
@@benbritton1389 Thank you sir. That was a huge help 🌷🌷🌷
Is it possible to give the links for the papers in the description, please?
The slide deck is linked in the playlist description (or you can find it on the techniques section of the group website, expmicromech.com).
@@benbritton1389 thanks
hi sir, is this analysis the quantitative or qualitative if we want to know in simple words?
Quantitative = putting numbers and precision, e.g. 20 at% Si +/- 1%. Qualitative = describing where the silicon is located, e.g. this is a silicon rich particle.
I’m suing you boy did you copy my bitchy friend
Thank you. 10 years after seeing first IPF maps I roughly understand what do they encode: red: flat, green: edge touching view plane at sharpest angle, blue: sharpest corner. To my excuse, I'm a software engineer that came to contact with EBSD just by accident and I sort of wondered if I can extract this from CTF files without storing like 6 image files (phase, 3x IPF, euler, quality, maybe something else). I have to realize it, red color is pretty obvious (if coloring is consistent among different software).
Hey - thanks for the comment. You can take the CTF data and convert it to the IPF colouring - this does depend on the symmetry of the crystal system and the specific IPF colour key you would like to use to represent orientations. These approaches are what the commercial software does internally, and also routines can be found in MTEX (and elsewhere!). You can find a paper exploring this by Gert Nolze and Ralf Hielscher: www.tu-chemnitz.de/mathematik/preprint/2016/PREPRINT_01.pdf
I have watched the entire series of the EBSD videos and it helped me a lot to understand the background in regards of the theory, experimental set-up und interpretation. Awesome work! However, this video simply ends without a proper outro. Is there none or did there happen anything wrong during the editing? Thanks a lot!
Hey - thanks for the comment. The series 'concludes' with the final video - ruclips.net/video/XWrxfFqlQvY/видео.html I will (hopefully, when I have time/teaching slows down a bit) add some more lectures to the series - I'm still thinking about what they should be!
Excellent presentation !!
Thank you very much for the review and I hope the series are useful!
Very Informative...
Thank you for this kind note!
This is the best introduction to EBSD I saw on youtube, thank you. Can you introduce the practice to really do these experiments and analysis procedures, like texture analysis, GOS analysis, KAM analysis, GND analysis . I have gone through some of your lectures, it really helps a lot! Can't wait to see more. (My research mainly focused on the microstructural characterization of additive manufactured superalloys.)
Thanks for your kind note, and note of encouragement. I'm just thinking of what topics to expand the series towards, and will consider a longer explore of different post processing areas.
Hi Ben, I am working on my master project and I try to describe the different reference/coordinate systems that are used in EBSD technique. With little research I realized that each software manufacturer uses slightly different terminology to describe their references frames. I wanted to ask you if In the cvideo on the 1:57 minute, the B slide that depicts the sample coordinates is the same as what is referred by others "crystal reference frame" or more specific the coordinate system RD-TD-ND? Thank you in advance and thanks for the well structures and complete videos about EBSD.
Hi - thanks for the comment and note. The axes systems shown at 1:57 are the detector (Subscript D), the sample (subscript S), the gnomonic/detector frame (subscript g,d). The crystal frame in this (Bruker based) convention has an additional crystal frame. This is much better described in: "Tutorial: Crystal orientations and EBSD - Or which way is up?" doi.org/10.1016/j.matchar.2016.04.008 (see the python and matlab codes, and also the supplementary document written by Dr Winkelmann for extra info!).
@@benbritton1389 ok thanks is clear now! So the the sample axes system is the same as what other refer as RD-TD-ND ( I am using the Aztec suite to produce my maps ) or it can be any coordinate system on the sample? I have read also the tutorial still I miss some of the details... Thanks again!
Hi - typically the RD-TD-ND notation is inherited from the fact that one of the manufacturers had a significant amount of work looking at rolled sheet of aluminium, and pointed the rolling direction down the sample (perpendicular to the tilt axis). This was subsequently encoded with RD as equivalent to 'X' in a rotation convention for the sample (and not crystal) coordinate system. As this early work was largely on cubic materials, the subtlety of the difference between the sample and crystal coordinate system was rarely explicitly mentioned/explored. This was also complicated as another major manufacturer originated with more of a geology start (ish) which has different conventions/ideas on this topic. The tutorial paper talks to establishing two major aspects - (1) how the pattern relates to the crystal within the sample (i.e. the sample frame and the crystal frame); (2) how the map relates to this frame (e.g. the scanning grid).
@@benbritton1389 ok perfect ! Now is clear thanks very much .
@@vangelisdialeismas3728 Awesome - happy to help where I can if you need something more! The tutorial paper has some handy code to plot simulated diffraction patterns overlaid with your own, which can be handy in addressing issues with regards to sample/crystal frame and the pattern. I'd recommend trying to do this with a sample of lower than cubic symmetry!
Just happen to stumble on Section 8 video, will watch the whole series. Great job explaining EBSD, I'm actually understanding , finally!
YAAY! This is awesome, and super pleased that you are finding this useful.
Thank you for your great work, Ben! I was enjoying watching your videos!
Thanks for the watching & the feedback Danyil!
This series videos are great, Doc! I was trying to find videos to explain EBSD clear and understandable. Here I found them! Thanks!
This is awesome - thank you for the kind feedback, and I hope they are handy!
Brilliant
Ah - that's very kind, thank you @YKeir
Hi Ben, this is a super helpful guide to EBSD. We met briefly several years ago; even though we never got the chance to work together, I am lucky to be able to learn from you in this way now that I'm starting out with my PhD. Thanks for uploading this series.
Hi James! It's lovely to hear from you, and I'm glad that you are starting out your PhD journey - best of luck, and thank you for the encouraging feedback.
Thanks Ben, excellent talk.
Ah - that's very kind, thanks Austin!
Hello Ben, I have a question that confused me for a long time. According to the Bragg's Law, the 2theta causing diffraction exists bcz of the relationship between the incident electron and the crystal plane. But as 2:41 shows the BSE beam and plane doesn't have a angle of theta. Is it because the incident electron which causes the diffraction is not actually the BSE beam showing in the picture? Thankss!
Hi - thanks for your query. In EBSD, the electron that diffracts is not the incoming incident electron beam, but instead a scattered electron. This means that the angle theta is between the plane trace (i.e. the centre of the band) and the band edge.
@@benbritton1389 Thank for this explanation!
Thanks for those videos. They are really helpful. I will also appreciate your videos on TEM techniques (with emphasis on structural materials). :)
Hi - thanks for the note. At the moment I'm focussing on SEM-based techniques I am afraid.
Very nice introduction of EBSD and its data processing skills. Thank you Ben.
This is a very kind comment, thanks! If there's anything you could suggest me going into for future videos, please let me know.
Thank you very much Ben. You are such a good person
@@benbritton1389 OK, thank you. I am very interested in such introduction or training since my research mainly focused on the microstructural characterization of metals, which always need EBSD measurement and related analysis.
Brilliant Ben! Love the knitted EBSP.
Thanks Austin. The titanium pattern (with indexed bands) was kindly crocheted by Dr Vivian Tong!
That's an impressive amount of crocheting.
Excellent introduction of EBSD.
Thank you!
Very good introduction to EBSD for who are studying materials science.
This is very kind feedback, thanks.